Technology Process of C21H20BClF2N2Si
There total 1 articles about C21H20BClF2N2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; triethylamine;
In
toluene;
at 65 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/ja309079f
- Guidance literature:
-
C21H20BClF2N2Si; 2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethanol;
With
copper(l) iodide;
In
dichloromethane;
for 0.166667h;
Inert atmosphere;
With
tetrabutyl ammonium fluoride;
In
dichloromethane;
at 0 ℃;
for 5h;
DOI:10.1039/c2cc38429a
- Guidance literature:
-
C21H20BClF2N2Si; (4-azidobutyl)triphenyl phosphonium bromide;
With
copper(l) iodide; tris[2-(dimethylamino)ethyl]amine;
In
dichloromethane;
for 0.5h;
Inert atmosphere;
With
tetrabutyl ammonium fluoride;
In
dichloromethane;
at 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1039/c6ob02407f
