C₁₃H₁₃N₃O₅S

Base Information

• Chemical Name: C₁₃H₁₃N₃O₅S
• CAS No.: 1380394-42-2
• Molecular Formula: C₁₃H₁₃N₃O₅S
• Molecular Weight: 323.329

Synonyms:C₁₃H₁₃N₃O₅S

Chemical Property of C₁₃H₁₃N₃O₅S

Chemical Property:

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Technology Process of C₁₃H₁₃N₃O₅S

There total 1 articles about C₁₃H₁₃N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2',3',5'-tri-O-acetyl-5-iodouridine (84500-33-4,65499-40-3) → C13H13N3O5S (1380394-42-2)

Guidance literature:

Multi-step reaction with 6 steps

1.1: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 80 °C

1.2: 80 °C

2.1: bromine / tetrachloromethane; 1,2-dichloro-ethane / 1.5 h / 0 °C

3.1: acetic anhydride; acetic acid; zinc / N,N-dimethyl-formamide / 4 h / 80 °C

4.1: triethylamine; p-toluenesulfonyl chloride / acetonitrile / 20 °C

5.1: ammonium hydroxide / acetonitrile / 72 h / 40 °C

6.1: copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine / N,N-dimethyl-formamide / 60 °C

With bis-triphenylphosphine-palladium(II) chloride; ammonium hydroxide; copper(l) iodide; bromine; acetic anhydride; caesium carbonate; acetic acid; triethylamine; p-toluenesulfonyl chloride; N,N`-dimethylethylenediamine; zinc; In tetrachloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; 1.1: Stille coupling / 1.2: Stille coupling;

DOI:10.1021/ol3012327

upstream raw materials:

2',3',5'-tri-O-acetyl-5-iodouridine

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