Spiro-piperidine)>-5'-hydroxy-6'-benzyl-7'-oxo

Base Information

Chemical Name:Spiro-piperidine)>-5'-hydroxy-6'-benzyl-7'-oxo
CAS No.:137646-45-8
Molecular Formula:C₁₉H₂₃NO₃
Molecular Weight:313.397
Hs Code.:

Spiro<cyclohexane-1,4'-(3'a,7'a-dihydrofuro<2,3-c>-piperidine)>-5'-hydroxy-6'-benzyl-7'-oxo

Synonyms:Spiro-piperidine)>-5'-hydroxy-6'-benzyl-7'-oxo

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Chemical Property of Spiro-piperidine)>-5'-hydroxy-6'-benzyl-7'-oxo

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Technology Process of Spiro-piperidine)>-5'-hydroxy-6'-benzyl-7'-oxo

There total 3 articles about Spiro-piperidine)>-5'-hydroxy-6'-benzyl-7'-oxo which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 79841-92-2
N-Cyclohexanylidene N-benzyl-2-amidofurane

: 137646-45-8
Spiro-piperidine)>-5'-hydroxy-6'-benzyl-7'-oxo

Guidance literature:: With water; In acetonitrile; for 5h; Irradiation;
DOI:10.1016/S0040-4020(01)89732-5

Reference yield:

: 527-69-5
2-furancarbonyl chloride

: 137646-45-8
Spiro-piperidine)>-5'-hydroxy-6'-benzyl-7'-oxo

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Et₃N / benzene / 15 h / Ambient temperature

2: 79 percent / water / acetonitrile / 5 h / Irradiation

With water; triethylamine; In acetonitrile; benzene;
DOI:10.1016/S0040-4020(01)89732-5

Reference yield:

: Benzyl-cyclohexylidenemethyl-amine

: 137646-45-8
Spiro-piperidine)>-5'-hydroxy-6'-benzyl-7'-oxo

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Et₃N / benzene / 15 h / Ambient temperature

2: 79 percent / water / acetonitrile / 5 h / Irradiation

With water; triethylamine; In acetonitrile; benzene;
DOI:10.1016/S0040-4020(01)89732-5