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Technology Process of (CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)(1+)*SbF6(1-)=[(CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)]SbF6

(CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)(1+)*SbF6(1-)=[(CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)]SbF6

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  • Chemical Name:(CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)(1+)*SbF6(1-)=[(CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)]SbF6
  • CAS No.:184219-44-1
  • Molecular Formula:C29H36CuN4*F6Sb
  • Molecular Weight:739.918
  • Hs Code.:
(CH<sub>2</sub>CH<sub>2</sub>)3N<sub>3</sub>(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)3Cu(CH<sub>3</sub>CN)<sup>(1+)</sup>*SbF<sub>6</sub><sup>(1-)</sup>=[(CH<sub>2</sub>CH<sub>2</sub>)3N<sub>3</sub>(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)3Cu(CH<sub>3</sub>CN)]SbF<sub>6</sub>

Synonyms:(CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)(1+)*SbF6(1-)=[(CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)]SbF6

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Chemical Property of (CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)(1+)*SbF6(1-)=[(CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)]SbF6
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Technology Process of (CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)(1+)*SbF6(1-)=[(CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)]SbF6

There total 1 articles about (CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)(1+)*SbF6(1-)=[(CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)]SbF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

[Cu(acetonitrile)4]SbF<sub>6</sub>
137436-76-1

[Cu(acetonitrile)4]SbF6

N,N',N''-tribenzyl-1,4,7-triazacyclononane
125262-43-3

N,N',N''-tribenzyl-1,4,7-triazacyclononane

(CH<sub>2</sub>CH<sub>2</sub>)3N<sub>3</sub>(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)3Cu(CH<sub>3</sub>CN)<sup>(1+)</sup>*SbF<sub>6</sub><sup>(1-)</sup>=[(CH<sub>2</sub>CH<sub>2</sub>)3N<sub>3</sub>(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)3Cu(CH<sub>3</sub>CN)]SbF<sub>6</sub>
184219-44-1

(CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)(1+)*SbF6(1-)=[(CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)]SbF6

Guidance literature:
In tetrahydrofuran; stirring (10 min), addn. of Et2O, filtration; recrystn. (THF/ether or CH2Cl2/ether); elem. anal.;
DOI:10.1021/ja962305c

Reference yield:

(CH<sub>2</sub>CH<sub>2</sub>)3N<sub>3</sub>(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)3Cu(CH<sub>3</sub>CN)<sup>(1+)</sup>*SbF<sub>6</sub><sup>(1-)</sup>=[(CH<sub>2</sub>CH<sub>2</sub>)3N<sub>3</sub>(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)3Cu(CH<sub>3</sub>CN)]SbF<sub>6</sub>
184219-44-1

(CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)(1+)*SbF6(1-)=[(CH2CH2)3N3(CH2C6H5)3Cu(CH3CN)]SbF6

oxygen
80937-33-3

oxygen

[Cu2(N,N',N''-tribenzyl-1,4,7-triazacyclononane)2(μ-oxo)2](SbF6)2

[Cu2(N,N',N''-tribenzyl-1,4,7-triazacyclononane)2(μ-oxo)2](SbF6)2

Guidance literature:
In dichloromethane; -80°C, bubbling of O2 (15 min); not isolated;
DOI:10.1021/ja962305c
upstream raw materials:

[Cu(acetonitrile)4]SbF6

N,N',N''-tribenzyl-1,4,7-triazacyclononane

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