S-(2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl) phenylacetothiohydroximate

Base Information

Chemical Name:S-(2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl) phenylacetothiohydroximate
CAS No.:174020-66-7
Molecular Formula:C₃₅H₃₁NO₈S
Molecular Weight:625.699
Hs Code.:

Synonyms:S-(2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl) phenylacetothiohydroximate

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Chemical Property of S-(2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl) phenylacetothiohydroximate

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Technology Process of S-(2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl) phenylacetothiohydroximate

There total 4 articles about S-(2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl) phenylacetothiohydroximate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 701-72-4
phenylacetohydroximoyl chloride

: 174020-62-3
2,3,6-tri-O-benzoyl-4-deoxy-1-thio-β-D-xylo-hexopyranose

: 174020-66-7
S-(2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl) phenylacetothiohydroximate

Guidance literature:: With triethylamine; In diethyl ether; dichloromethane; for 1h; Ambient temperature;
DOI:10.1016/0008-6215(95)00265-0

Reference yield:

: 155155-55-8
2,3,6-tri-O-benzoyl-4-deoxy-α-D-xylo-hexopyranosyl bromide

: 174020-66-7
S-(2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl) phenylacetothiohydroximate

Guidance literature:: Multi-step reaction with 3 steps

1: acetone / 1 h / Heating

2: aq. K₂S₂O₅ / CH₂Cl₂ / 0.5 h / Heating

3: 98 percent / triethylamine / diethyl ether; CH₂Cl₂ / 1 h / Ambient temperature

With potassium disulphite; triethylamine; In diethyl ether; dichloromethane; acetone;
DOI:10.1016/0008-6215(95)00265-0

Reference yield:

: 151073-09-5
1,2,3,6-tetra-O-benzoyl-4-deoxy-α-D-xylo-hexopyranose

: 174020-66-7
S-(2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl) phenylacetothiohydroximate

Guidance literature:: Multi-step reaction with 4 steps

1: HBr / CH₂Cl₂; acetic acid / 1 h / Ambient temperature

2: acetone / 1 h / Heating

3: aq. K₂S₂O₅ / CH₂Cl₂ / 0.5 h / Heating

4: 98 percent / triethylamine / diethyl ether; CH₂Cl₂ / 1 h / Ambient temperature

With potassium disulphite; hydrogen bromide; triethylamine; In diethyl ether; dichloromethane; acetic acid; acetone;
DOI:10.1016/0008-6215(95)00265-0