pentafluorophenolato(triphenylphosphine)gold

Base Information

Chemical Name:pentafluorophenolato(triphenylphosphine)gold
CAS No.:121589-52-4
Molecular Formula:C₂₄H₁₅AuF₅OP
Molecular Weight:642.315
Hs Code.:

Synonyms:pentafluorophenolato(triphenylphosphine)gold

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Chemical Property of pentafluorophenolato(triphenylphosphine)gold

Chemical Property:

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Technology Process of pentafluorophenolato(triphenylphosphine)gold

There total 1 articles about pentafluorophenolato(triphenylphosphine)gold which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.2%

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 4615-85-4
potassium perfluorophenolate

: 121589-52-4
pentafluorophenolato(triphenylphosphine)gold

Guidance literature:: In tetrahydrofuran; dichloromethane; byproducts: KCl; all manipulations under N2 or Ar atm.; Au compd. dissolved in CH2Cl2, soln. of K compd. in THF added, stirred for several h; solvent removed in vac., solid dissolved in CH2Cl2, filtered, concd. layered with hexane, recrystd.; elem. anal.;
DOI:10.1016/j.poly.2005.06.012

Reference yield:

: 121589-52-4
pentafluorophenolato(triphenylphosphine)gold

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 771-61-9
2,3,4,5,6-pentafluorophenol

Guidance literature:: With hydrogenchloride; In hydrogenchloride; addn. of 0.1 N HCl to soln. of Au-complex, stirring (2 min); solvent removal (vac.), extn. of pentafluorophenol from solid residue by ether; ppt. dissoln. in chloroform, salting out by petroleum ether;

Reference yield:

: 121589-52-4
pentafluorophenolato(triphenylphosphine)gold

: 14243-64-2
(triphenylphosphine)gold(I) chloride

Guidance literature:: With hydrogenchloride; sodium chloride; In water; toluene; byproducts: F5C6ONa; addn. of satd. aq. soln. of NaCl to soln. of Au-complex (THF), stirring (at least 20 min); addn. of water, titration with HCl; benzene addn., org. layer sepn., washing (water), drying (K2CO3), salting out by petroleum ether;