Technology Process of C23H25N3OSSi
There total 2 articles about C23H25N3OSSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium carbonate;
bis-triphenylphosphine-palladium(II) chloride;
In
ethanol; water; toluene;
at 130 ℃;
for 0.0833333h;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen / palladium 10% on activated carbon / ethanol / 4 h
2: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C
3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 5 h
4: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / ethanol; water; toluene / 0.08 h / 130 °C / Microwave irradiation
With
hydrogenchloride; hydrogen; sodium carbonate; sodium nitrite;
bis-triphenylphosphine-palladium(II) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon;
In
ethanol; water; toluene;
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
for 1h;