3-nitrobenzenecarboperoxoic acid

Base Information

• Chemical Name: 3-nitrobenzenecarboperoxoic acid
• CAS No.: 2453-41-0
• Molecular Formula: C7H5 N O5
• Molecular Weight: 183.12
• Mol file: 2453-41-0.mol

Synonyms:Peroxybenzoicacid, m-nitro- (7CI,8CI); 3-Nitroperoxybenzoic acid; m-Nitroperbenzoic acid;m-Nitroperoxybenzoic acid

Chemical Property of 3-nitrobenzenecarboperoxoic acid

Chemical Property:

• Vapor Pressure: 1.07E-05mmHg at 25°C
• Boiling Point: 356.3°C at 760 mmHg
• Flash Point: 169.3°C
• PSA: 92.35000
• Density: 1.523g/cm³
• LogP: 1.74780

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-nitrobenzenecarboperoxoic acid

There total 3 articles about 3-nitrobenzenecarboperoxoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

3-nitrobenzoic acid (121-92-6) → 3-nitroperbenzoic acid (2453-41-0)

Guidance literature:

With potassium peroxomonosulphate; N-benzyl-N,N,N-triethylammonium chloride; In diethyl ether; water; at 20 ℃; for 15h;

Reference yield:

bis-(3-nitro-benzoyl)-peroxide (904-58-5) → 3-nitroperbenzoic acid (2453-41-0)

Guidance literature:

With chloroform; sodium methylate; Versetzen des Reaktionsgemisches mit kaltem Wasser und Ansaeurern der erhaltenen wss. Loesung mit wss. Schwefelsaeure;

DOI:10.1039/jr9550001525

Reference yield:

→ 3-nitroperbenzoic acid (2453-41-0)

Guidance literature:

nach Vilkas, Bl.1959,1401;

DOI:10.1039/j29660000675

upstream raw materials:

bis-(3-nitro-benzoyl)-peroxide

3-nitrobenzoic acid

Downstream raw materials:

3,3'-dinitro-1,1'-biphenyl

3′-nitro[1,1′-biphenyl]-3-carboxylic acid

3'-nitro-biphenyl-4-carboxylic acid

C₂₀H₁₃IN₂O₁₀

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