3-Chloro-benzenesulfonic acid 3-(toluene-4-sulfonyl)-propyl ester

Base Information

• Chemical Name: 3-Chloro-benzenesulfonic acid 3-(toluene-4-sulfonyl)-propyl ester
• CAS No.: 82777-15-9
• Molecular Formula: C₁₆H₁₇ClO₅S₂
• Molecular Weight: 388.893
• Mol file: 82777-15-9.mol

Synonyms:3-Chloro-benzenesulfonic acid 3-(toluene-4-sulfonyl)-propyl ester

Chemical Property of 3-Chloro-benzenesulfonic acid 3-(toluene-4-sulfonyl)-propyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-Chloro-benzenesulfonic acid 3-(toluene-4-sulfonyl)-propyl ester

There total 3 articles about 3-Chloro-benzenesulfonic acid 3-(toluene-4-sulfonyl)-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

3-Chloro-benzenesulfonic acid 3-p-tolylsulfanyl-propyl ester (82777-19-3) → 3-Chloro-benzenesulfonic acid 3-(toluene-4-sulfonyl)-propyl ester (82777-15-9)

Guidance literature:

With ammonium molybdate; dihydrogen peroxide; In methanol;

DOI:10.1039/P29820000579

Reference yield:

3-[(4-methylphenyl)sulfanyl]-1-propanol (3147-28-2) → 3-Chloro-benzenesulfonic acid 3-(toluene-4-sulfonyl)-propyl ester (82777-15-9)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine

2: 50 percent / 30 percent aq. hydrogen peroxide, ammonium molybdate / methanol

With ammonium molybdate; dihydrogen peroxide; In pyridine; methanol;

DOI:10.1039/P29820000579

Reference yield:

3-chlorophenylsulfonyl chloride (2888-06-4) → 3-Chloro-benzenesulfonic acid 3-(toluene-4-sulfonyl)-propyl ester (82777-15-9)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine

2: 50 percent / 30 percent aq. hydrogen peroxide, ammonium molybdate / methanol

With ammonium molybdate; dihydrogen peroxide; In pyridine; methanol;

DOI:10.1039/P29820000579

upstream raw materials:

3-Chloro-benzenesulfonic acid 3-p-tolylsulfanyl-propyl ester

3-[(4-methylphenyl)sulfanyl]-1-propanol

3-chlorophenylsulfonyl chloride

Downstream raw materials:

cyclopropyl p-tolyl sulphone