ethyl 5-tert-butyl-3-{[5-tert-butyl-3-(pivaloylamino)-2-hydroxybenzoyl]amino}-2-hydroxybenzoate

Base Information

Chemical Name:ethyl 5-tert-butyl-3-{[5-tert-butyl-3-(pivaloylamino)-2-hydroxybenzoyl]amino}-2-hydroxybenzoate
CAS No.:849363-21-9
Molecular Formula:C₂₉H₄₀N₂O₆
Molecular Weight:512.646
Hs Code.:

Synonyms:ethyl 5-tert-butyl-3-{[5-tert-butyl-3-(pivaloylamino)-2-hydroxybenzoyl]amino}-2-hydroxybenzoate

Suppliers and Price of ethyl 5-tert-butyl-3-{[5-tert-butyl-3-(pivaloylamino)-2-hydroxybenzoyl]amino}-2-hydroxybenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl 5-tert-butyl-3-{[5-tert-butyl-3-(pivaloylamino)-2-hydroxybenzoyl]amino}-2-hydroxybenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl 5-tert-butyl-3-{[5-tert-butyl-3-(pivaloylamino)-2-hydroxybenzoyl]amino}-2-hydroxybenzoate

There total 6 articles about ethyl 5-tert-butyl-3-{[5-tert-butyl-3-(pivaloylamino)-2-hydroxybenzoyl]amino}-2-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 849362-94-3
ethyl 5-tert-butyl-3-amino-2-hydroxybenzoate

: 849362-96-5
5-tert-butyl-2-hydroxy-3-(pivaloylamino)benzoic acid

: 849363-21-9
ethyl 5-tert-butyl-3-{[5-tert-butyl-3-(pivaloylamino)-2-hydroxybenzoyl]amino}-2-hydroxybenzoate

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃;
DOI:10.1002/anie.200461842

Reference yield:

: 849362-93-2
ethyl 5-tert-butyl-2-hydroxy-3-nitrobenzoate

: 849363-21-9
ethyl 5-tert-butyl-3-{[5-tert-butyl-3-(pivaloylamino)-2-hydroxybenzoyl]amino}-2-hydroxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / hydrogen / Pd/C / methanol / 2 h

2: 69 percent / DCC / tetrahydrofuran / 20 °C

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1002/anie.200461842

Reference yield:

: 118-61-6
2-hydroxy-benzoic acid ethyl ester

: 849363-21-9
ethyl 5-tert-butyl-3-{[5-tert-butyl-3-(pivaloylamino)-2-hydroxybenzoyl]amino}-2-hydroxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: aluminium trichloride / CH₂Cl₂ / 3 h / Heating

2: 9.6 g / fuming HNO₃; acetic acid / 0.17 h / 40 °C

3: 74 percent / hydrogen / Pd/C / methanol / 2 h

4: 69 percent / DCC / tetrahydrofuran / 20 °C

With aluminium trichloride; hydrogen; nitric acid; acetic acid; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/anie.200461842