Technology Process of C28H31F5O8
There total 12 articles about C28H31F5O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 2 steps
1: NaClO2; NaH2PO4; 2-methyl-2-butene / 2-methyl-propan-2-ol; H2O / 1.5 h / 25 °C
2: 115 mg / dicyclohexylcarbodiimide / CH2Cl2 / 2.5 h / 25 °C
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; dicyclohexyl-carbodiimide;
In
dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ja054748z
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 94 percent / oxalyl chloride; dimethyl sulfoxide; Et3N / CH2Cl2 / -78 - 20 °C
2: NaClO2; NaH2PO4; 2-methyl-2-butene / 2-methyl-propan-2-ol; H2O / 1.5 h / 25 °C
3: 115 mg / dicyclohexylcarbodiimide / CH2Cl2 / 2.5 h / 25 °C
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide;
In
dichloromethane; water; tert-butyl alcohol;
1: Swern oxidation;
DOI:10.1021/ja054748z