7-{(1R,2R)-2-[3-(4-Amino-3-iodo-phenyl)-propylamino]-cyclopentyl}-heptanoic acid

Base Information

Chemical Name:7-{(1R,2R)-2-[3-(4-Amino-3-iodo-phenyl)-propylamino]-cyclopentyl}-heptanoic acid
CAS No.:107539-84-4
Molecular Formula:C₂₁H₃₃IN₂O₂
Molecular Weight:472.41
Hs Code.:

Synonyms:7-{(1R,2R)-2-[3-(4-Amino-3-iodo-phenyl)-propylamino]-cyclopentyl}-heptanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-{(1R,2R)-2-[3-(4-Amino-3-iodo-phenyl)-propylamino]-cyclopentyl}-heptanoic acid

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Technology Process of 7-{(1R,2R)-2-[3-(4-Amino-3-iodo-phenyl)-propylamino]-cyclopentyl}-heptanoic acid

There total 5 articles about 7-{(1R,2R)-2-[3-(4-Amino-3-iodo-phenyl)-propylamino]-cyclopentyl}-heptanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 107539-79-7,107539-80-0
dl-16-(4'-aminophenyl)-17,18,19,20-tetranor-13-azaprostanoic acid

: 107539-84-4
7-{(1R,2R)-2-[3-(4-Amino-3-iodo-phenyl)-propylamino]-cyclopentyl}-heptanoic acid

Guidance literature:: With sodium acetate buffer; chloroamine-T; sodium iodide; In methanol; for 0.166667h;
DOI:10.1021/jm00388a029

Reference yield:

: 37617-17-7
2-(6-methoxycarbonylhexyl)-cyclopentanone

: 107539-84-4
7-{(1R,2R)-2-[3-(4-Amino-3-iodo-phenyl)-propylamino]-cyclopentyl}-heptanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) 4A molecular sieves, 2.) NaBH₄ / 1.) methanol, 24 h, 2.) methanol, 30 min

2: 96 percent / H₂ / 10percent Pd/C / ethanol / 1810.02 Torr / Ambient temperature

3: 80 percent / 2.5percent aq. NaOH / 4 h / Heating

4: 50 percent / sodium acetate buffer, sodium iodide, chloramine-T / methanol / 0.17 h

With sodium hydroxide; sodium tetrahydroborate; sodium acetate buffer; 4 A molecular sieve; hydrogen; chloroamine-T; sodium iodide; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jm00388a029

Reference yield:

: 80258-61-3
3-(4-nitrophenyl)propan-1-amine

: 107539-84-4
7-{(1R,2R)-2-[3-(4-Amino-3-iodo-phenyl)-propylamino]-cyclopentyl}-heptanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) 4A molecular sieves, 2.) NaBH₄ / 1.) methanol, 24 h, 2.) methanol, 30 min

2: 96 percent / H₂ / 10percent Pd/C / ethanol / 1810.02 Torr / Ambient temperature

3: 80 percent / 2.5percent aq. NaOH / 4 h / Heating

4: 50 percent / sodium acetate buffer, sodium iodide, chloramine-T / methanol / 0.17 h

With sodium hydroxide; sodium tetrahydroborate; sodium acetate buffer; 4 A molecular sieve; hydrogen; chloroamine-T; sodium iodide; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jm00388a029