4-(3,3,4,4,5,5,6,6-octafluoroazepan-1-yl)-N-((pyridin-4-yl)methylene)benzenamine

Base Information

• Chemical Name: 4-(3,3,4,4,5,5,6,6-octafluoroazepan-1-yl)-N-((pyridin-4-yl)methylene)benzenamine
• CAS No.: 1415593-57-5
• Molecular Formula: C₁₈H₁₃F₈N₃
• Molecular Weight: 423.309

Synonyms:4-(3,3,4,4,5,5,6,6-octafluoroazepan-1-yl)-N-((pyridin-4-yl)methylene)benzenamine

Chemical Property of 4-(3,3,4,4,5,5,6,6-octafluoroazepan-1-yl)-N-((pyridin-4-yl)methylene)benzenamine

Chemical Property:

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Technology Process of 4-(3,3,4,4,5,5,6,6-octafluoroazepan-1-yl)-N-((pyridin-4-yl)methylene)benzenamine

There total 2 articles about 4-(3,3,4,4,5,5,6,6-octafluoroazepan-1-yl)-N-((pyridin-4-yl)methylene)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.98%

pyridine-4-carbaldehyde (872-85-5) + 4-(3,3,4,4,5,5,6,6-octafluoroazepan-1-yl)benzenamine (1415593-53-1) → 4-(3,3,4,4,5,5,6,6-octafluoroazepan-1-yl)-N-((pyridin-4-yl)methylene)benzenamine (1415593-57-5)

Guidance literature:

With magnesium sulfate; In dichloromethane; at 20 ℃;

DOI:10.1016/j.jfluchem.2012.07.009

Reference yield:

trifluoromethanesulfonic acid 2,2,3,3,4,4,5,5-octafluoro-1,6-hexanediyl ester (51437-76-4) → 4-(3,3,4,4,5,5,6,6-octafluoroazepan-1-yl)-N-((pyridin-4-yl)methylene)benzenamine (1415593-57-5)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / ethanol / 30 h / Reflux

2: magnesium sulfate / dichloromethane / 20 °C

With magnesium sulfate; triethylamine; In ethanol; dichloromethane;

DOI:10.1016/j.jfluchem.2012.07.009

Reference yield: 53.0%

4-(3,3,4,4,5,5,6,6-octafluoroazepan-1-yl)-N-((pyridin-4-yl)methylene)benzenamine (1415593-57-5) + 1-Bromooctadecane (112-89-0) → C36H50F8N3(1+)*Br(1-) (1415593-69-9)

Guidance literature:

In acetonitrile; for 12h; Reflux;

DOI:10.1016/j.jfluchem.2012.07.009

upstream raw materials:

pyridine-4-carbaldehyde

4-(3,3,4,4,5,5,6,6-octafluoroazepan-1-yl)benzenamine

trifluoromethanesulfonic acid 2,2,3,3,4,4,5,5-octafluoro-1,6-hexanediyl ester

Downstream raw materials:

C₃₂H₄₂F₈N₃⁽¹⁺⁾*Br^(1-)

C₃₄H₄₆F₈N₃⁽¹⁺⁾*Br^(1-)

C₃₆H₅₀F₈N₃⁽¹⁺⁾*Br^(1-)

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