4-O-benzyl-2-O-levulinoy1-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

Base Information

Chemical Name:4-O-benzyl-2-O-levulinoy1-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate
CAS No.:1349064-68-1
Molecular Formula:C₂₈H₃₂Cl₃NO₈
Molecular Weight:616.923
Hs Code.:

Synonyms:4-O-benzyl-2-O-levulinoy1-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

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Chemical Property of 4-O-benzyl-2-O-levulinoy1-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

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Technology Process of 4-O-benzyl-2-O-levulinoy1-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

There total 2 articles about 4-O-benzyl-2-O-levulinoy1-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1448429-77-3
allyl 4-O-benzyl-2-O-levulinoyl-3-O-p-methoxybenzyl-α-L-rhamnopyranoside

: 545-06-2
trichloroacetonitrile

: 1349064-68-1
4-O-benzyl-2-O-levulinoy1-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

: 1448430-13-4
4-O-benzyl-2-O-levulinoy1-3-O-para-methoxybenzyl-β-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,2-dichloro-ethane; at 20 ℃; Overall yield = 97 %; Overall yield = 12.66 g; Inert atmosphere;

Reference yield:

: C₂₆H₃₂O₈

: 545-06-2
trichloroacetonitrile

: 1349064-68-1
4-O-benzyl-2-O-levulinoy1-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

: 1448430-13-4
4-O-benzyl-2-O-levulinoy1-3-O-para-methoxybenzyl-β-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,2-dichloro-ethane; at 20 ℃; for 0.333333h; Overall yield = 97 %; Overall yield = 12.66 g; Inert atmosphere;
DOI:10.1002/ejoc.201300180

Reference yield: 91.0%

: 1349064-68-1
4-O-benzyl-2-O-levulinoy1-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

: 1603827-12-8
C₇₂H₇₆Cl₃NO₁₆

: 1603827-11-7
allyl (4-O-benzyl-3-O-para-methoxybenzyl-2-O-levulinoyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→4)-(benzyl 2,3-di-O-benzyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Guidance literature:: 4-O-benzyl-2-O-levulinoy1-3-O-para-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate; C₇₂H₇₆Cl₃NO₁₆; In toluene; at 20 ℃; for 1h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In toluene; at -10 ℃; for 0.5h;