C₄₁H₅₀O₆Si

Base Information

Chemical Name:C₄₁H₅₀O₆Si
CAS No.:1413374-02-3
Molecular Formula:C₄₁H₅₀O₆Si
Molecular Weight:666.93
Hs Code.:

C<sub>41</sub>H<sub>50</sub>O<sub>6</sub>Si

Synonyms:C₄₁H₅₀O₆Si

Suppliers and Price of C₄₁H₅₀O₆Si

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of C₄₁H₅₀O₆Si

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of C₄₁H₅₀O₆Si

There total 12 articles about C₄₁H₅₀O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1413373-99-5
C₄₁H₅₂O₆Si

: 1413374-02-3
C₄₁H₅₀O₆Si

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 1413374-02-3
C₄₁H₅₀O₆Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: toluene; tetrahydrofuran / 3.67 h / 0 - 50 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -78 - -40 °C / Inert atmosphere

2.2: 2.25 h / -78 - 20 °C

3.1: L-proline / dimethyl sulfoxide / 8 h / 50 °C

4.1: pyridine; trichlorophosphate / 0 - 20 °C

5.1: cerium(III) chloride heptahydrate / tetrahydrofuran; methanol / 0.5 h / -23 °C

5.2: 0.75 h

6.1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

6.2: 12 h / 40 °C

7.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.2: 2 h / 0 - 20 °C

8.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; oxalyl dichloride; cerium(III) chloride heptahydrate; dimethylsulfide borane complex; Dess-Martin periodane; dimethyl sulfoxide; L-proline; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 13096-62-3
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 1413374-02-3
C₄₁H₅₀O₆Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 - 0 °C

1.3: cooling with ice

2.1: sodium tetrahydroborate / tetrahydrofuran / 20 °C

3.1: trifluoroacetic anhydride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C

3.2: -78 - 0 °C

4.1: potassium carbonate / 18-crown-6 ether / toluene / 20 °C

5.1: cerium(III) chloride heptahydrate / tetrahydrofuran; methanol / 0.5 h / -23 °C

5.2: 0.75 h

6.1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

6.2: 12 h / 40 °C

7.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.2: 2 h / 0 - 20 °C

8.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; n-butyllithium; cerium(III) chloride heptahydrate; dimethylsulfide borane complex; potassium carbonate; Dess-Martin periodane; dimethyl sulfoxide; trifluoroacetic anhydride; 18-crown-6 ether; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;