Technology Process of 2,3,3',4-tetramethoxy-5'-<(1-phenyl-1H-5-tetrazolyl)oxy>-1,1'-biphenyl
There total 6 articles about 2,3,3',4-tetramethoxy-5'-<(1-phenyl-1H-5-tetrazolyl)oxy>-1,1'-biphenyl which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
for 16h;
Ambient temperature;
DOI:10.1002/hlca.19880710531
- Guidance literature:
-
Multi-step reaction with 5 steps
1: NaOMe / methanol / 2 h / Heating
2: 1.) 20percent NaOH; 2.) conc. HCl / 1.) 120 deg C, 4 h; 2.) 120 deg C, 1 h
3: 96 percent / conc. H2SO4 / 39 h / Ambient temperature
4: 83.6 percent / Hg(OAc)2 / acetic acid / 4.5 h / Heating
5: 87.8 percent / K2CO3 / dimethylformamide / 16 h / Ambient temperature
With
hydrogenchloride; sodium hydroxide; sulfuric acid; mercury(II) diacetate; sodium methylate; potassium carbonate;
In
methanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19880710531
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 96 percent / conc. H2SO4 / 39 h / Ambient temperature
2: 83.6 percent / Hg(OAc)2 / acetic acid / 4.5 h / Heating
3: 87.8 percent / K2CO3 / dimethylformamide / 16 h / Ambient temperature
With
sulfuric acid; mercury(II) diacetate; potassium carbonate;
In
acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19880710531