N-{2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-2-diphenylphosphanyl-terephthalamic acid methyl ester

Base Information

Chemical Name:N-{2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-2-diphenylphosphanyl-terephthalamic acid methyl ester
CAS No.:868394-26-7
Molecular Formula:C₂₇H₃₁N₂O₅P
Molecular Weight:494.527
Hs Code.:

<i>N</i>-{2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-2-diphenylphosphanyl-terephthalamic acid methyl ester

Synonyms:N-{2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-2-diphenylphosphanyl-terephthalamic acid methyl ester

Suppliers and Price of N-{2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-2-diphenylphosphanyl-terephthalamic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-{2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-2-diphenylphosphanyl-terephthalamic acid methyl ester

Chemical Property:

Purity/Quality:: >95.00% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-{2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-2-diphenylphosphanyl-terephthalamic acid methyl ester

There total 2 articles about N-{2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-2-diphenylphosphanyl-terephthalamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 929-59-9,892154-56-2
3,6-dioxa-1,8-diaminooctane

: 532931-48-9
2-(diphenylphosphanyl)terephthalic acid 1-methyl ester 4-(N-succinimidyl) ester

: 868394-26-7
N-{2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-2-diphenylphosphanyl-terephthalamic acid methyl ester

Guidance literature:: In tetrahydrofuran; water; N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1021/ol035635s

Reference yield:

: 361154-31-6
3-(diphenylphosphino)-4-(methoxycarbonyl)benzoic acid

: 868394-26-7
N-{2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-2-diphenylphosphanyl-terephthalamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: diisopropylethylamine / tetrahydrofuran; dimethylformamide; H₂O / 1 h / 20 °C

2: tetrahydrofuran; dimethylformamide; H₂O / 2 h / 20 °C

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/ol035635s

Reference yield: 60.0%

: N-[1,10]phenanthrolin-4-ylmethyl-succinamic acid; compound with triethyl-amine

: 868394-26-7
N-{2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-2-diphenylphosphanyl-terephthalamic acid methyl ester

: 2-diphenylphosphanyl-N-(2-{2-[2-(1,10-phenanthrolin-4-oxobutanamido)ethoxy]ethoxy}ethyl)terephthalamic acid methyl ester

Guidance literature:: N-[1,10]phenanthrolin-4-ylmethyl-succinamic acid; compound with triethyl-amine; With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; for 0.75h;

N-{2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-2-diphenylphosphanyl-terephthalamic acid methyl ester; In N,N-dimethyl-formamide;
DOI:10.1021/ja054128y