C₃₉H₅₄O₈SSi

Base Information

Chemical Name:C₃₉H₅₄O₈SSi
CAS No.:1282034-29-0
Molecular Formula:C₃₉H₅₄O₈SSi
Molecular Weight:711.004
Hs Code.:

C<sub>39</sub>H<sub>54</sub>O<sub>8</sub>SSi

Synonyms:C₃₉H₅₄O₈SSi

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Chemical Property of C₃₉H₅₄O₈SSi

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Technology Process of C₃₉H₅₄O₈SSi

There total 4 articles about C₃₉H₅₄O₈SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1282034-45-0
C₃₃H₄₀O₈S

: 69739-34-0
t-butyldimethylsiyl triflate

: 1282034-29-0
C₃₉H₅₄O₈SSi

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/anie.201006035

Reference yield:

: 273749-60-3
phenyl 4,6-O-(4-methoxybenzylidene)-1-thio-β-D-glucopyranoside

: 1282034-29-0
C₃₉H₅₄O₈SSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: di(n-butyl)tin oxide / toluene / 12 h / Reflux; Dean-Stark apparatus

1.2: 12 h / 80 °C

2.1: pyridine; dmap / 18 h / 70 °C / Inert atmosphere

3.1: sodium cyanoborohydride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere; Molecular sieve

3.2: 0 °C / Inert atmosphere

4.1: 2,6-dimethylpyridine / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; dmap; di(n-butyl)tin oxide; sodium cyanoborohydride; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.201006035

Reference yield:

: 1282034-43-8
C₂₈H₃₀O₇S

: 1282034-29-0
C₃₉H₅₄O₈SSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine; dmap / 18 h / 70 °C / Inert atmosphere

2.1: sodium cyanoborohydride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere; Molecular sieve

2.2: 0 °C / Inert atmosphere

3.1: 2,6-dimethylpyridine / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; dmap; sodium cyanoborohydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201006035