{OsCl(1-phenyl 3,4-dimethylphosphole)(NCCH₃)(CO)(triphenylphosphine)2}ClO₄

Base Information

Chemical Name:{OsCl(1-phenyl 3,4-dimethylphosphole)(NCCH₃)(CO)(triphenylphosphine)2}ClO₄
CAS No.:133361-59-8
Molecular Formula:C₅₁H₄₆ClNOOsP₃*ClO₄
Molecular Weight:1106.96
Hs Code.:

{OsCl(1-phenyl 3,4-dimethylphosphole)(NCCH<sub>3</sub>)(CO)(triphenylphosphine)2}ClO<sub>4</sub>

Synonyms:{OsCl(1-phenyl 3,4-dimethylphosphole)(NCCH₃)(CO)(triphenylphosphine)2}ClO₄

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Chemical Property of {OsCl(1-phenyl 3,4-dimethylphosphole)(NCCH₃)(CO)(triphenylphosphine)2}ClO₄

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Technology Process of {OsCl(1-phenyl 3,4-dimethylphosphole)(NCCH₃)(CO)(triphenylphosphine)2}ClO₄

There total 1 articles about {OsCl(1-phenyl 3,4-dimethylphosphole)(NCCH₃)(CO)(triphenylphosphine)2}ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 133361-57-6
OsHCl(1-phenyl 3,4-dimethylphosphole)(CO)(triphenylphosphine)2

: 75-05-8,26809-02-9
acetonitrile

: 133361-59-8
{OsCl(1-phenyl 3,4-dimethylphosphole)(NCCH₃)(CO)(triphenylphosphine)2}ClO₄

Guidance literature:: With HClO₄; H₂O; In dichloromethane; acetonitrile; byproducts: H2; treatment of Os-complex with aq.HClO4 in a soln. of CH2Cl2/CH3CN (1:1), react. for 2 h; mixture of isomers; evapn., recrystn. from CH2Cl2/C2H5OH/isopropanol; elem. anal.;
DOI:10.1016/0022-328X(91)86251-K

Reference yield: 98.0%

: 133361-59-8
{OsCl(1-phenyl 3,4-dimethylphosphole)(NCCH₃)(CO)(triphenylphosphine)2}ClO₄

: 133346-63-1,133442-80-5
OsCl₂(1-phenyl 3,4-dimethylphosphole)(CO)(triphenylphosphine)2

Guidance literature:: With LiCl; In ethanol; dichloromethane; byproducts: CH3CN; dissoln. of Os-complex and LiCl in CH2C2/C2H5OH (1:1), 2 h react. (ppt.); mixture of cis/trans isomers (Cl ligands); addn. of C2H5OH, evapn. (vac.), filtration, successive washes with H2O, C2H5OH, n-hexane; elem. anal.;
DOI:10.1016/0022-328X(91)86251-K

Reference yield: 91.0%

: 133361-59-8
{OsCl(1-phenyl 3,4-dimethylphosphole)(NCCH₃)(CO)(triphenylphosphine)2}ClO₄

: 133361-60-1
Os(N₃)Cl(1-phenyl 3,4-dimethylphosphole)(CO)(triphenylphosphine)2

Guidance literature:: With NaN₃; In ethanol; dichloromethane; byproducts: CH3CN, NaClO4; dissoln. of Os-complex and NaN3 in CH2Cl2/C2H5OH (1:1), react. for 1 h; evapn. (vac.), filtation, successive washes with H2, C2H5OH, n-hexane; elem. anal.;
DOI:10.1016/0022-328X(91)86251-K