C₄₉H₆₆N₄O₁₉Si

Base Information

Chemical Name:C₄₉H₆₆N₄O₁₉Si
CAS No.:204992-97-2
Molecular Formula:C₄₉H₆₆N₄O₁₉Si
Molecular Weight:1043.16
Hs Code.:

C<sub>49</sub>H<sub>66</sub>N<sub>4</sub>O<sub>19</sub>Si

Synonyms:C₄₉H₆₆N₄O₁₉Si

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Chemical Property of C₄₉H₆₆N₄O₁₉Si

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Technology Process of C₄₉H₆₆N₄O₁₉Si

There total 8 articles about C₄₉H₆₆N₄O₁₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 204992-96-1
C₆₃H₇₄N₄O₂₁SSi

: 204992-97-2
C₄₉H₆₆N₄O₁₉Si

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 1h;
DOI:10.1021/ja9740071

Reference yield:

: 58871-10-6
3,4-di-O-benzyl-D-glucal

: 204992-97-2
C₄₉H₆₆N₄O₁₉Si

Guidance literature:: Multi-step reaction with 6 steps

1: ZnCl₂ / tetrahydrofuran; diethyl ether

2: 82 percent / collidine, DMAP / 2.5 h / Ambient temperature

3: 83 percent / iodonium bis(sym-collidine) perchlorate, 3 Angstroem molecular sieves / tetrahydrofuran / 0.92 h / -10 - 0 °C

4: 85 percent / tetrabutylammonium azide / tetrahydrofuran / 0.67 h / Ambient temperature

5: 90 percent / DMAP / tetrahydrofuran / 1 h / Ambient temperature

6: 91 percent / iPr₂NEt / tetrahydrofuran / 1 h

With 2,3,5-trimethyl-pyridine; dmap; iodonium(di-γ-collidine) perchlorate; 3 A molecular sieve; tetrabutylammoniun azide; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja9740071

Reference yield:

: (3aR,4R,7aR)-4-((3aS,4R,6R,7R,7aR)-7-Hydroxy-2-oxo-4-triisopropylsilanyloxymethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxymethyl)-3a,7a-dihydro-4H-[1,3]dioxolo[4,5-c]pyran-2-one

: 204992-97-2
C₄₉H₆₆N₄O₁₉Si

Guidance literature:: Multi-step reaction with 7 steps

1: dimethyldioxirane / CH₂Cl₂; acetone / 0.5 h

2: ZnCl₂ / tetrahydrofuran; diethyl ether

3: 82 percent / collidine, DMAP / 2.5 h / Ambient temperature

4: 83 percent / iodonium bis(sym-collidine) perchlorate, 3 Angstroem molecular sieves / tetrahydrofuran / 0.92 h / -10 - 0 °C

5: 85 percent / tetrabutylammonium azide / tetrahydrofuran / 0.67 h / Ambient temperature

6: 90 percent / DMAP / tetrahydrofuran / 1 h / Ambient temperature

7: 91 percent / iPr₂NEt / tetrahydrofuran / 1 h

With 2,3,5-trimethyl-pyridine; dmap; iodonium(di-γ-collidine) perchlorate; 3 A molecular sieve; 3,3-dimethyldioxirane; tetrabutylammoniun azide; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; In tetrahydrofuran; diethyl ether; dichloromethane; acetone;
DOI:10.1021/ja9740071