[α,β-(13)C2]styrene oxide

Base Information

• Chemical Name: [α,β-(13)C2]styrene oxide
• CAS No.: 1189532-69-1
• Molecular Formula: C₈H₈O
• Molecular Weight: 122.129
• Mol file: 1189532-69-1.mol

Synonyms:[α,β-(13)C2]styrene oxide

Chemical Property of [α,β-(13)C2]styrene oxide

Chemical Property:

Purity/Quality:

>98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [α,β-(13)C2]styrene oxide

There total 1 articles about [α,β-(13)C2]styrene oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

styrene-α, β-13C2 (31124-36-4) → [α,β-(13)C2]styrene oxide (1189532-69-1)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; Cooling with ice;

DOI:10.1002/chem.200900834

Reference yield: 25.0%

[α,β-(13)C2]styrene oxide (1189532-69-1) → (S)-[α,β-(13)C2]styrene oxide (1189532-70-4)

Guidance literature:

With (acetao)(aqua)(S,S)-N,N′-bis(3,5-di-tert-butylsalicylidene-1,2-cyclohexanediamino)-cobalt(III); water; In tetrahydrofuran; optical yield given as %ee; Resolution of racemate;

DOI:10.1002/chem.200900834

Reference yield:

[α,β-(13)C2]styrene oxide (1189532-69-1) → C6(13)C2H7LiO

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In [D₈]THF; at 173 ℃;

DOI:10.1002/chem.200900834

upstream raw materials:

styrene-α, β-¹³C₂

Downstream raw materials:

(S)-[α,β-(13)C2]styrene oxide