(R)-methyl-3-(5-methoxypyridin-2-ylamino)-2-(oxirane-2-ylmethoxy)benzoate

Base Information

Chemical Name:(R)-methyl-3-(5-methoxypyridin-2-ylamino)-2-(oxirane-2-ylmethoxy)benzoate
CAS No.:1334176-46-3
Molecular Formula:C₁₇H₁₈N₂O₅
Molecular Weight:330.34
Hs Code.:

Synonyms:(R)-methyl-3-(5-methoxypyridin-2-ylamino)-2-(oxirane-2-ylmethoxy)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-methyl-3-(5-methoxypyridin-2-ylamino)-2-(oxirane-2-ylmethoxy)benzoate

Chemical Property:

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Technology Process of (R)-methyl-3-(5-methoxypyridin-2-ylamino)-2-(oxirane-2-ylmethoxy)benzoate

There total 4 articles about (R)-methyl-3-(5-methoxypyridin-2-ylamino)-2-(oxirane-2-ylmethoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1334176-45-2
methyl-2-hydroxy-3-(5-methoxypyridin-2-ylamino)benzoate

: 115314-14-2,115314-17-5
(R)-glycidyl nosylate

: 1334176-46-3
(R)-methyl-3-(5-methoxypyridin-2-ylamino)-2-(oxirane-2-ylmethoxy)benzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

Reference yield:

: 942615-04-5
2-((2-methoxyethoxy)methoxy)-3-nitrobenzoic acid methyl ester

: 1334176-46-3
(R)-methyl-3-(5-methoxypyridin-2-ylamino)-2-(oxirane-2-ylmethoxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / 5%-palladium/activated carbon / methanol / 24 h / 20 °C

2: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / 1,4-dioxane / 12 h / 90 °C

3: hydrogenchloride; water / methanol / 0.5 h / 40 °C

4: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

With hydrogenchloride; water; hydrogen; potassium carbonate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; 5%-palladium/activated carbon; palladium diacetate; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;

Reference yield:

: 942615-05-6
3-amino-2-((2-methoxyethoxy)methoxy)benzoic acid methyl ester

: 1334176-46-3
(R)-methyl-3-(5-methoxypyridin-2-ylamino)-2-(oxirane-2-ylmethoxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / 1,4-dioxane / 12 h / 90 °C

2: hydrogenchloride; water / methanol / 0.5 h / 40 °C

3: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

With hydrogenchloride; water; potassium carbonate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;