ethyl (3R,7aS,11aS)-3-phenyl-5-thioxo-2,3,5,6,7,7a,10,11-octahydrooxazolo[2,3-j]quinoline-8-butyrate

Base Information

Chemical Name:ethyl (3R,7aS,11aS)-3-phenyl-5-thioxo-2,3,5,6,7,7a,10,11-octahydrooxazolo[2,3-j]quinoline-8-butyrate
CAS No.:1227923-14-9
Molecular Formula:C₂₃H₂₉NO₃S
Molecular Weight:399.554
Hs Code.:

Synonyms:ethyl (3R,7aS,11aS)-3-phenyl-5-thioxo-2,3,5,6,7,7a,10,11-octahydrooxazolo[2,3-j]quinoline-8-butyrate

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Chemical Property of ethyl (3R,7aS,11aS)-3-phenyl-5-thioxo-2,3,5,6,7,7a,10,11-octahydrooxazolo[2,3-j]quinoline-8-butyrate

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Technology Process of ethyl (3R,7aS,11aS)-3-phenyl-5-thioxo-2,3,5,6,7,7a,10,11-octahydrooxazolo[2,3-j]quinoline-8-butyrate

There total 1 articles about ethyl (3R,7aS,11aS)-3-phenyl-5-thioxo-2,3,5,6,7,7a,10,11-octahydrooxazolo[2,3-j]quinoline-8-butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1040735-63-4
ethyl (3R,7aS,11aS)-5-oxo-3-phenyl-2,3,5,6,7,7a,10,11-octahydrooxazolo[2,3-j]quinoline-8-butyrate

: 1227923-14-9
ethyl (3R,7aS,11aS)-3-phenyl-5-thioxo-2,3,5,6,7,7a,10,11-octahydrooxazolo[2,3-j]quinoline-8-butyrate

Guidance literature:: With Lawessons reagent; In benzene; for 3h; Reflux; Inert atmosphere;
DOI:10.1021/jo1005894

Reference yield: 74.0%

: 1227923-14-9
ethyl (3R,7aS,11aS)-3-phenyl-5-thioxo-2,3,5,6,7,7a,10,11-octahydrooxazolo[2,3-j]quinoline-8-butyrate

: 96-32-2
bromoacetic acid methyl ester

: ethyl (3R,7aS,11aS)-5-(methoxycarbonylmethylene)-3-phenyl-2,3,5,6,7,7a,10,11-octahydrooxazolo[2,3-j]quinoline-8-butyrate

Guidance literature:: ethyl (3R,7aS,11aS)-3-phenyl-5-thioxo-2,3,5,6,7,7a,10,11-octahydrooxazolo[2,3-j]quinoline-8-butyrate; bromoacetic acid methyl ester; In chloroform; at 20 ℃; for 17h; Inert atmosphere; Darkness;

With triethylamine; phosphorous acid trimethyl ester; In chloroform; for 24h; Reflux; Inert atmosphere;
DOI:10.1021/jo1005894