N-octyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine

Base Information

Chemical Name:N-octyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine
CAS No.:828268-98-0
Molecular Formula:C₂₅H₄₁NO₄
Molecular Weight:419.605
Hs Code.:

Synonyms:N-octyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-octyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine

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Technology Process of N-octyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine

There total 1 articles about N-octyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 111-86-4
n-Octylamine

: 157609-12-6
1,2-anhydro-6-O-benzyl-3,4-O-isopropylidene-5a-carba-α-D-galactopyranose

: 828268-98-0
N-octyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine

Guidance literature:: In isopropyl alcohol; at 120 ℃; for 48h;
DOI:10.1016/j.bmc.2004.09.023

Reference yield: 82.0%

: 828268-98-0
N-octyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine

: 108-24-7
acetic anhydride

: 828268-99-1
Acetic acid (3aS,4S,5R,7R,7aS)-5-(acetyl-octyl-amino)-7-benzyloxymethyl-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-4-yl ester

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1016/j.bmc.2004.09.023

Reference yield:

: 828268-98-0
N-octyl-6-O-benzyl-3,4-O-isopropylidene-5a-carba-β-D-galactopyranosylamine

: N-octyl-5a-carba-β-D-galactopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / pyridine / 20 °C

2: 71 percent / hydrochloric acid / 6 h / 120 °C

With pyridine; hydrogenchloride;
DOI:10.1016/j.bmc.2004.09.023