Technology Process of 4,4’-bis(hexylphenyl)benzophenone
There total 5 articles about 4,4’-bis(hexylphenyl)benzophenone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetone;
for 48h;
Reflux;
DOI:10.1139/V10-056
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trichlorophosphate; zinc(II) chloride / 1,2-dichloro-benzene / 2 h / 65 - 70 °C
2: ammonium hydroxide / 3 h / 10 - 20 °C
3: aluminum (III) chloride / carbon disulfide / 6 h / Reflux
4: potassium carbonate; tetrabutylammomium bromide / acetone / 48 h / Reflux
With
aluminum (III) chloride; ammonium hydroxide; tetrabutylammomium bromide; potassium carbonate; zinc(II) chloride; trichlorophosphate;
In
carbon disulfide; 1,2-dichloro-benzene; acetone;
3: |Fries Phenol Ester Rearrangement / 4: |Williamson Ether Synthesis;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: cyclohexane / 2 h / 30 - 40 °C
2: trichlorophosphate; zinc(II) chloride / 1,2-dichloro-benzene / 2 h / 65 - 70 °C
3: ammonium hydroxide / 3 h / 10 - 20 °C
4: aluminum (III) chloride / carbon disulfide / 6 h / Reflux
5: potassium carbonate; tetrabutylammomium bromide / acetone / 48 h / Reflux
With
aluminum (III) chloride; ammonium hydroxide; tetrabutylammomium bromide; potassium carbonate; zinc(II) chloride; trichlorophosphate;
In
carbon disulfide; cyclohexane; 1,2-dichloro-benzene; acetone;
4: |Fries Phenol Ester Rearrangement / 5: |Williamson Ether Synthesis;