5-[4-(O₂-methyl diazen-1-ium-1,2-diolato)phenyl]-1-(4-sulfamoylphenyl)-3-trifluoromethyl-1H-pyrazole

Base Information

• Chemical Name: 5-[4-(O₂-methyl diazen-1-ium-1,2-diolato)phenyl]-1-(4-sulfamoylphenyl)-3-trifluoromethyl-1H-pyrazole
• CAS No.: 1245272-96-1
• Molecular Formula: C₁₇H₁₄F₃N₅O₄S
• Molecular Weight: 441.39
• Mol file: 1245272-96-1.mol

Synonyms:5-[4-(O₂-methyl diazen-1-ium-1,2-diolato)phenyl]-1-(4-sulfamoylphenyl)-3-trifluoromethyl-1H-pyrazole

Chemical Property of 5-[4-(O₂-methyl diazen-1-ium-1,2-diolato)phenyl]-1-(4-sulfamoylphenyl)-3-trifluoromethyl-1H-pyrazole

Chemical Property:

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Technology Process of 5-[4-(O₂-methyl diazen-1-ium-1,2-diolato)phenyl]-1-(4-sulfamoylphenyl)-3-trifluoromethyl-1H-pyrazole

There total 1 articles about 5-[4-(O₂-methyl diazen-1-ium-1,2-diolato)phenyl]-1-(4-sulfamoylphenyl)-3-trifluoromethyl-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

5-[4-(O2-ammonium diazen-1-ium-1,2-diolato)phenyl]-1-(4-sulfamoylphenyl)-3-trifluoromethyl-1H-pyrazole + dimethyl sulfate (77-78-1) → 5-[4-(O2-methyl diazen-1-ium-1,2-diolato)phenyl]-1-(4-sulfamoylphenyl)-3-trifluoromethyl-1H-pyrazole (1245272-96-1)

Guidance literature:

With sodium carbonate; In methanol; at 0 - 25 ℃; Inert atmosphere;

DOI:10.1016/j.bmcl.2010.06.022

upstream raw materials:

dimethyl sulfate