15-(4-hydroxyphenyl)pentadec-12-enal

Base Information

• Chemical Name: 15-(4-hydroxyphenyl)pentadec-12-enal
• CAS No.: 1191914-16-5
• Molecular Formula: C₂₁H₃₂O₂
• Molecular Weight: 316.484
• Mol file: 1191914-16-5.mol

Synonyms:15-(4-hydroxyphenyl)pentadec-12-enal

Chemical Property of 15-(4-hydroxyphenyl)pentadec-12-enal

Chemical Property:

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Technology Process of 15-(4-hydroxyphenyl)pentadec-12-enal

There total 1 articles about 15-(4-hydroxyphenyl)pentadec-12-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

4-(15-hydroxypentadec-3-enyl)phenol (1191914-15-4) → 15-(4-hydroxyphenyl)pentadec-12-enal (1191914-16-5)

Guidance literature:

4-(15-hydroxypentadec-3-enyl)phenol; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.416667h; Inert atmosphere;

With triethylamine; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1021/ja904792q

Reference yield: 69.0%

15-(4-hydroxyphenyl)pentadec-12-enal (1191914-16-5) + (5-carboxypentyl)triphenylphosphonium bromide (50889-29-7) → 21-(4-hydroxyphenyl)henixosa-6,18-dienoic acid (1191914-17-6)

Guidance literature:

(5-carboxypentyl)triphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at -10 ℃; for 0.25h; Inert atmosphere;

15-(4-hydroxyphenyl)pentadec-12-enal; In tetrahydrofuran; at -10 ℃; for 2.5h; Inert atmosphere;

DOI:10.1021/ja904792q

upstream raw materials:

4-(15-hydroxypentadec-3-enyl)phenol

Downstream raw materials:

21-(4-hydroxyphenyl)henixosa-6,18-dienoic acid