6',7-bis(benzoyloxy)-2',4'-dimethoxy-3'-(3-methyl-2-butenyl)isoflavone

Base Information

• Chemical Name: 6',7-bis(benzoyloxy)-2',4'-dimethoxy-3'-(3-methyl-2-butenyl)isoflavone
• CAS No.: 89966-12-1
• Molecular Formula: C₃₆H₃₀O₈
• Molecular Weight: 590.629
• Mol file: 89966-12-1.mol

Synonyms:6',7-bis(benzoyloxy)-2',4'-dimethoxy-3'-(3-methyl-2-butenyl)isoflavone

Chemical Property of 6',7-bis(benzoyloxy)-2',4'-dimethoxy-3'-(3-methyl-2-butenyl)isoflavone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6',7-bis(benzoyloxy)-2',4'-dimethoxy-3'-(3-methyl-2-butenyl)isoflavone

There total 5 articles about 6',7-bis(benzoyloxy)-2',4'-dimethoxy-3'-(3-methyl-2-butenyl)isoflavone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

2-methyl-3-buten-2-ol (115-18-4) + 6',7-bis(benzoyloxy)-2',4'-dimethoxyisoflavone (89966-11-0) → 6',7-bis(benzoyloxy)-2',4'-dimethoxy-3'-(3-methyl-2-butenyl)isoflavone (89966-12-1) + 6',7-bis(benzoyloxy)-2',4'-dimethoxy-5'-(3-methyl-2-butenyl)isoflavone (89966-13-2)

Guidance literature:

Reference yield:

6',7-bis(benzyloxy)-2',4'-dimethoxyisoflavone (89966-04-1) → 6',7-bis(benzoyloxy)-2',4'-dimethoxy-3'-(3-methyl-2-butenyl)isoflavone (89966-12-1)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / methanol; ethyl acetate

2: pyridine / 63 °C

3: 12 percent

With pyridine; hydrogen; palladium on activated charcoal; In methanol; ethyl acetate;

Reference yield:

6',7-dihydroxy-2',4'-dimethoxyisoflavone (89966-05-2) → 6',7-bis(benzoyloxy)-2',4'-dimethoxy-3'-(3-methyl-2-butenyl)isoflavone (89966-12-1)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 63 °C

2: 12 percent

With pyridine;

upstream raw materials:

2-methyl-3-buten-2-ol

6',7-bis(benzoyloxy)-2',4'-dimethoxyisoflavone

benzoyl chloride

6',7-dihydroxy-2',4'-dimethoxyisoflavone

Downstream raw materials:

licoricone

6',7-diacetoxy-2',4'-dimethoxy-3'-(3-methyl-2-butenyl)isoflavone

2',4',6',7-tetramethoxy-3'-(3-methyl-2-butenyl)isoflavone