1-[4,4-dimethyl-2-(1-oxy(diphenylphosphino)-1-methyl)]-4,5-dihydrooxazole

Base Information

Chemical Name:1-[4,4-dimethyl-2-(1-oxy(diphenylphosphino)-1-methyl)]-4,5-dihydrooxazole
CAS No.:932015-63-9
Molecular Formula:C₁₈H₂₀NO₂P
Molecular Weight:313.336
Hs Code.:

Synonyms:1-[4,4-dimethyl-2-(1-oxy(diphenylphosphino)-1-methyl)]-4,5-dihydrooxazole

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Chemical Property of 1-[4,4-dimethyl-2-(1-oxy(diphenylphosphino)-1-methyl)]-4,5-dihydrooxazole

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Technology Process of 1-[4,4-dimethyl-2-(1-oxy(diphenylphosphino)-1-methyl)]-4,5-dihydrooxazole

There total 1 articles about 1-[4,4-dimethyl-2-(1-oxy(diphenylphosphino)-1-methyl)]-4,5-dihydrooxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 86354-11-2
(4,4-dimethyl-4,5-dihydrooxazolyl-2-yl)methanol

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 932015-63-9
1-[4,4-dimethyl-2-(1-oxy(diphenylphosphino)-1-methyl)]-4,5-dihydrooxazole

Guidance literature:: With n-butyllithium; In hexane; toluene; at -78 ℃; for 2h;
DOI:10.1039/b616962g

Reference yield: 92.0%

: 932015-63-9
1-[4,4-dimethyl-2-(1-oxy(diphenylphosphino)-1-methyl)]-4,5-dihydrooxazole

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 958889-53-7
(1-[4,4-dimethyl-2-(1-oxy(diphenylphosphino)-1-methyl)]-4,5-dihydrooxazole)cobalt dichloride

Guidance literature:: In tetrahydrofuran; under inert atmosphere; CoCl2 added to soln. of ligand in THF; stirred at room temp. for 15 h; solvent removed under reduced pressure; washed with Et2O; filtered; ppt.dried under vac.; elem. anal.;
DOI:10.1039/b706818b

Reference yield: 79.0%

: 932015-63-9
1-[4,4-dimethyl-2-(1-oxy(diphenylphosphino)-1-methyl)]-4,5-dihydrooxazole

: chloromethyl(1,5-cyclooctadiene)palladium(II)

: 932015-65-1
PdClCH₃(CH₃)2C₃H₂NOCOP(C₆H₅)2H₂

Guidance literature:: In dichloromethane; (under N2, Schlenk); Pd-complex added to CH2Cl2 soln. of ligand at room temp., stirred overnight; solvent evapd. under reduced pressure, ppt. washed with Et2O, pentane, dried under vac.; elem. anal.;
DOI:10.1039/b616962g