C₃₁H₄₅F₃N₂O₁₃

Base Information

Chemical Name:C₃₁H₄₅F₃N₂O₁₃
CAS No.:1448451-79-3
Molecular Formula:C₃₁H₄₅F₃N₂O₁₃
Molecular Weight:710.699
Hs Code.:

C<sub>31</sub>H<sub>45</sub>F<sub>3</sub>N<sub>2</sub>O<sub>13</sub>

Synonyms:C₃₁H₄₅F₃N₂O₁₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₄₅F₃N₂O₁₃

Chemical Property:

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Technology Process of C₃₁H₄₅F₃N₂O₁₃

There total 5 articles about C₃₁H₄₅F₃N₂O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28746-78-3
17-chloro-3,6,9,12,15-pentaoxaheptadecan-1-ol

: 1448451-79-3
C₃₁H₄₅F₃N₂O₁₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium azide / N,N-dimethyl-formamide / 15 h / 75 °C

2.1: N-iodo-succinimide; triethylsilyl trifluoromethyl sulfonate / dichloromethane / 1 h / -20 °C / Molecular sieve

3.1: ethylenediamine; i-Amyl alcohol / 4 h / 140 °C / Reflux

4.1: pyridine / 1.5 h / Reflux

5.1: sodium methylate / methanol / 16 h

5.2: 5 h / 40 °C

6.1: triethylamine / methanol / 3 h

6.2: 16 h

With pyridine; N-iodo-succinimide; sodium azide; i-Amyl alcohol; triethylsilyl trifluoromethyl sulfonate; sodium methylate; ethylenediamine; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide; 5.2: |Staudinger Azide Reduction;
DOI:10.1016/j.tetlet.2013.06.065

Reference yield:

: 1448451-77-1
C₃₅H₄₄N₄O₁₃

: 1448451-79-3
C₃₁H₄₅F₃N₂O₁₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: ethylenediamine; i-Amyl alcohol / 4 h / 140 °C / Reflux

2.1: pyridine / 1.5 h / Reflux

3.1: sodium methylate / methanol / 16 h

3.2: 5 h / 40 °C

4.1: triethylamine / methanol / 3 h

4.2: 16 h

With pyridine; i-Amyl alcohol; sodium methylate; ethylenediamine; triethylamine; In methanol; 3.2: |Staudinger Azide Reduction;
DOI:10.1016/j.tetlet.2013.06.065

Reference yield:

: 86770-69-6
17-azido-3,6,9,12,15-pentaoxaheptadecan-1-ol

: 1448451-79-3
C₃₁H₄₅F₃N₂O₁₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-iodo-succinimide; triethylsilyl trifluoromethyl sulfonate / dichloromethane / 1 h / -20 °C / Molecular sieve

2.1: ethylenediamine; i-Amyl alcohol / 4 h / 140 °C / Reflux

3.1: pyridine / 1.5 h / Reflux

4.1: sodium methylate / methanol / 16 h

4.2: 5 h / 40 °C

5.1: triethylamine / methanol / 3 h

5.2: 16 h

With pyridine; N-iodo-succinimide; i-Amyl alcohol; triethylsilyl trifluoromethyl sulfonate; sodium methylate; ethylenediamine; triethylamine; In methanol; dichloromethane; 4.2: |Staudinger Azide Reduction;
DOI:10.1016/j.tetlet.2013.06.065