2-methyl-3-phenyl-5-<(phenylsulfonyl)methyl>-5-(phenylsulfonyl)isoxazolidine

Base Information

Chemical Name:2-methyl-3-phenyl-5-<(phenylsulfonyl)methyl>-5-(phenylsulfonyl)isoxazolidine
CAS No.:118171-20-3
Molecular Formula:C₂₃H₂₃NO₅S₂
Molecular Weight:457.571
Hs Code.:

Synonyms:2-methyl-3-phenyl-5-<(phenylsulfonyl)methyl>-5-(phenylsulfonyl)isoxazolidine

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Chemical Property of 2-methyl-3-phenyl-5-<(phenylsulfonyl)methyl>-5-(phenylsulfonyl)isoxazolidine

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Technology Process of 2-methyl-3-phenyl-5-<(phenylsulfonyl)methyl>-5-(phenylsulfonyl)isoxazolidine

There total 5 articles about 2-methyl-3-phenyl-5-<(phenylsulfonyl)methyl>-5-(phenylsulfonyl)isoxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 3376-23-6,7372-59-0,59862-60-1
C-phenyl-N-methylnitrone

: 2525-55-5
(prop-2-ene-1,2-diyldisulfonyl)dibenzene

: 118171-20-3
2-methyl-3-phenyl-5-<(phenylsulfonyl)methyl>-5-(phenylsulfonyl)isoxazolidine

Guidance literature:: In benzene; at 80 ℃; for 48h;
DOI:10.1021/jo00265a018

Reference yield: 79.0%

: 3376-23-6
N-methyl-α-phenylnitrone

: 2525-55-5
(prop-2-ene-1,2-diyldisulfonyl)dibenzene

: 117620-29-8,118171-20-3
(3S,5R)-5-Benzenesulfonyl-5-benzenesulfonylmethyl-2-methyl-3-phenyl-isoxazolidine

Guidance literature:: at 80 ℃; for 96h;
DOI:10.1016/S0040-4039(00)80070-2

Reference yield:

: 2525-40-8
prop-2-ynylsulfonylbenzene

: 117620-29-8,118171-20-3
(3S,5R)-5-Benzenesulfonyl-5-benzenesulfonylmethyl-2-methyl-3-phenyl-isoxazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / triethylamine / methanol / 24 h / Ambient temperature

2: 80 percent / hydrogen peroxide / acetic acid / 1 h / 80 °C

3: 79 percent / 96 h / 80 °C

With dihydrogen peroxide; triethylamine; In methanol; acetic acid;
DOI:10.1016/S0040-4039(00)80070-2