Technology Process of 2-(3-azidophenyl)-4,4,5,5-tetramethyl-2H-imidazoline-1-oxide-3-oxyl
There total 6 articles about 2-(3-azidophenyl)-4,4,5,5-tetramethyl-2H-imidazoline-1-oxide-3-oxyl which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium periodate;
In
dichloromethane; water;
for 0.0833333h;
DOI:10.1021/jo049500r
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: H2 / Pd/C / ethanol; tetrahydrofuran / 3 h / 2585.74 Torr
2.1: sulfuric acid; acetic acid; sodium nitrite / 0.25 h
2.2: sodium azide; water / 0.5 h
3.1: Et3N / methanol / 42 h
4.1: 58 percent / NaIO4 / CH2Cl2; H2O / 0.08 h
With
sodium periodate; sulfuric acid; hydrogen; acetic acid; triethylamine; sodium nitrite;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water;
DOI:10.1021/jo049500r
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 69 percent / p-toluenesulfonic acid / benzene / 3 h / Heating
2.1: H2 / Pd/C / ethanol; tetrahydrofuran / 3 h / 2585.74 Torr
3.1: sulfuric acid; acetic acid; sodium nitrite / 0.25 h
3.2: sodium azide; water / 0.5 h
4.1: Et3N / methanol / 42 h
5.1: 58 percent / NaIO4 / CH2Cl2; H2O / 0.08 h
With
sodium periodate; sulfuric acid; hydrogen; toluene-4-sulfonic acid; acetic acid; triethylamine; sodium nitrite;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; benzene;
DOI:10.1021/jo049500r
