(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOC₂H₅))⁽¹⁺⁾*PF₆^(1-) = [(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOC₂H₅))](PF₆)

Base Information

• Chemical Name: (C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOC₂H₅))⁽¹⁺⁾*PF₆^(1-) = [(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOC₂H₅))](PF₆)
• CAS No.: 174737-90-7
• Molecular Formula: C₂₆H₃₂CoO₃*F₆P
• Molecular Weight: 596.496

Synonyms:(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOC₂H₅))⁽¹⁺⁾*PF₆^(1-) = [(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOC₂H₅))](PF₆)

Chemical Property of (C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOC₂H₅))⁽¹⁺⁾*PF₆^(1-) = [(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOC₂H₅))](PF₆)

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Technology Process of (C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOC₂H₅))⁽¹⁺⁾*PF₆^(1-) = [(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOC₂H₅))](PF₆)

There total 1 articles about (C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOC₂H₅))⁽¹⁺⁾*PF₆^(1-) = [(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOC₂H₅))](PF₆) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

ammonium hexafluorophosphate + pentamethylcyclopentadienyllithium (51905-34-1) + Ethyl 2-ethoxy-4-phenyl-1,3-cyclopentadiene-1-carboxylate (136848-45-8) + cobalt acetylacetonate → (C5(CH3)5)Co(C5H2(OC2H5)(C6H5)(COOC2H5))(1+)*PF6(1-) = [(C5(CH3)5)Co(C5H2(OC2H5)(C6H5)(COOC2H5))](PF6) (174737-90-7)

Guidance literature:

With NaH; aq. HCl; In tetrahydrofuran; (N2 or Ar); stirring (room temp., 24 h), pouring over aq. HCl, addn. NH4PF6 to aq. layer.; recrystn. (MeOH); elem. anal.;

DOI:10.1246/bcsj.69.17

Reference yield: 95.0%

ammonium hexafluorophosphate + (C5(CH3)5)Co(C5H2(OC2H5)(C6H5)(COOC2H5))(1+)*PF6(1-) = [(C5(CH3)5)Co(C5H2(OC2H5)(C6H5)(COOC2H5))](PF6) (174737-90-7) → (C5(CH3)5)Co(C5H2(OC2H5)(C6H5)(COOH))(1+)*PF6(1-) = [(C5(CH3)5)Co(C5H2(OC2H5)(C6H5)(COOH))](PF6) (174737-94-1)

Guidance literature:

With NaH; aq. HCl; In hydrogenchloride; (N2 or Ar); stirring (80°C, 24 h), addn. of NH4PF6; recrystn. (EtOH); elem. anal.;

DOI:10.1246/bcsj.69.17

upstream raw materials:

pentamethylcyclopentadienyllithium

Ethyl 2-ethoxy-4-phenyl-1,3-cyclopentadiene-1-carboxylate

Downstream raw materials:

(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOH))⁽¹⁺⁾*PF₆^(1-) = [(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOH))](PF₆)

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