S-(+)-N-p-toluenesulfonyl-6-[2-tert-butyldimethylsilyloxyethylamino]-1-heptene

Base Information

Chemical Name:S-(+)-N-p-toluenesulfonyl-6-[2-tert-butyldimethylsilyloxyethylamino]-1-heptene
CAS No.:246229-16-3
Molecular Formula:C₂₂H₃₉NO₃SSi
Molecular Weight:425.708
Hs Code.:

Synonyms:S-(+)-N-p-toluenesulfonyl-6-[2-tert-butyldimethylsilyloxyethylamino]-1-heptene

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Chemical Property of S-(+)-N-p-toluenesulfonyl-6-[2-tert-butyldimethylsilyloxyethylamino]-1-heptene

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Technology Process of S-(+)-N-p-toluenesulfonyl-6-[2-tert-butyldimethylsilyloxyethylamino]-1-heptene

There total 3 articles about S-(+)-N-p-toluenesulfonyl-6-[2-tert-butyldimethylsilyloxyethylamino]-1-heptene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 246229-15-2
(S)-N-(hept-6-en-2-yl)-4-methylbenzenesulfonamide

: 86864-60-0
2-(tert-butyldimethylsilyloxy)ethyl bromide

: 246229-16-3
S-(+)-N-p-toluenesulfonyl-6-[2-tert-butyldimethylsilyloxyethylamino]-1-heptene

Guidance literature:: (S)-N-(hept-6-en-2-yl)-4-methylbenzenesulfonamide; With sodium hydride; In DMF (N,N-dimethyl-formamide); at 0 - 20 ℃; for 1.5h;

2-(tert-butyldimethylsilyloxy)ethyl bromide; In DMF (N,N-dimethyl-formamide); at 0 - 20 ℃; for 80h;

Reference yield:

: 119461-40-4
S-(+)-2-methyl-N-p-tosylaziridine

: 246229-16-3
S-(+)-N-p-toluenesulfonyl-6-[2-tert-butyldimethylsilyloxyethylamino]-1-heptene

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(l) iodide / diethyl ether / 4 h / -70 - 20 °C

2.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 1.5 h / 0 - 20 °C

2.2: 80 h / 0 - 20 °C

With copper(l) iodide; sodium hydride; In DMF (N,N-dimethyl-formamide); diethyl ether;

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 246229-16-3
S-(+)-N-p-toluenesulfonyl-6-[2-tert-butyldimethylsilyloxyethylamino]-1-heptene

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium borohydride; chloro-trimethyl-silane / trifluoroacetic acid

2.1: copper(l) iodide / diethyl ether / 4 h / -70 - 20 °C

3.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 1.5 h / 0 - 20 °C

3.2: 80 h / 0 - 20 °C

With copper(l) iodide; lithium borohydride; chloro-trimethyl-silane; sodium hydride; In DMF (N,N-dimethyl-formamide); diethyl ether; trifluoroacetic acid;