trimesitylfluorogermane

Base Information

• Chemical Name: trimesitylfluorogermane
• CAS No.: 136948-88-4
• Molecular Formula: C₂₇H₃₃FGe
• Molecular Weight: 449.147

Synonyms:trimesitylfluorogermane

Chemical Property of trimesitylfluorogermane

Chemical Property:

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Technology Process of trimesitylfluorogermane

There total 1 articles about trimesitylfluorogermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

trimesitylmethoxygermane (129044-57-1) → trimesitylfluorogermane (136948-88-4)

Guidance literature:

With hydrogen fluoride; In tetrahydrofuran; byproducts: methanol; (Ar or N2), dry solvents; addn. of excess of HF (40%) to a soln. of the Ge-compd. in THF, stirring at 30°C (30 min);; extn. (benzene), drying (Na2SO4, 12 h), concn. (reduced pressure), redissolving (THF), drying (Na2SO4, 2 h), concn. (reduced pressure), crystn. (pentane); elem. anal.;;

upstream raw materials:

trimesitylmethoxygermane

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