N₁-(2-methyl-6-(4-methylpiperazin-1-yl)pyrimidin-4-yl)benzene-1,3-diamine

Base Information

Chemical Name:N₁-(2-methyl-6-(4-methylpiperazin-1-yl)pyrimidin-4-yl)benzene-1,3-diamine
CAS No.:1402747-84-5
Molecular Formula:C₁₆H₂₂N₆
Molecular Weight:298.391
Hs Code.:

N<sub>1</sub>-(2-methyl-6-(4-methylpiperazin-1-yl)pyrimidin-4-yl)benzene-1,3-diamine

Synonyms:N₁-(2-methyl-6-(4-methylpiperazin-1-yl)pyrimidin-4-yl)benzene-1,3-diamine

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Chemical Property of N₁-(2-methyl-6-(4-methylpiperazin-1-yl)pyrimidin-4-yl)benzene-1,3-diamine

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Technology Process of N₁-(2-methyl-6-(4-methylpiperazin-1-yl)pyrimidin-4-yl)benzene-1,3-diamine

There total 5 articles about N₁-(2-methyl-6-(4-methylpiperazin-1-yl)pyrimidin-4-yl)benzene-1,3-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1402747-83-4
2-methyl-6-(4-methylpiperazin-1-yl)-N-(3-nitrophenyl)pyrimidin-4-amine

: 1402747-84-5
N₁-(2-methyl-6-(4-methylpiperazin-1-yl)pyrimidin-4-yl)benzene-1,3-diamine

Guidance literature:: With iron; ammonium chloride; In tetrahydrofuran; ethanol; water; for 2h; Reflux;
DOI:10.1111/cbdd.12198

Reference yield:

: 109-01-3
1-methyl-piperazine

: 1402747-84-5
N₁-(2-methyl-6-(4-methylpiperazin-1-yl)pyrimidin-4-yl)benzene-1,3-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium iodide / dimethyl sulfoxide / 0.5 h / 140 - 150 °C

2: iron; ammonium chloride / water; ethanol; tetrahydrofuran / 2 h / Reflux

With iron; ammonium chloride; potassium iodide; In tetrahydrofuran; ethanol; water; dimethyl sulfoxide;
DOI:10.1111/cbdd.12198

Reference yield:

: 1402747-70-9
6-chloro-2-methyl-N-(3-nitrophenyl)pyrimidin-4-amine hydrochloride

: 1402747-84-5
N₁-(2-methyl-6-(4-methylpiperazin-1-yl)pyrimidin-4-yl)benzene-1,3-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: dimethyl sulfoxide / 0.5 h / 140 - 150 °C

2: iron; ammonium chloride; hydrogenchloride / water; tetrahydrofuran / 2 h / Reflux

With hydrogenchloride; iron; ammonium chloride; In tetrahydrofuran; water; dimethyl sulfoxide;