2-amino-N,N,N′,N′-tetramethylisophthalamide

Base Information

Chemical Name:2-amino-N,N,N′,N′-tetramethylisophthalamide
CAS No.:57053-10-8
Molecular Formula:C₁₂H₁₇N₃O₂
Molecular Weight:235.286
Hs Code.:

Synonyms:2-amino-N,N,N′,N′-tetramethylisophthalamide

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Chemical Property of 2-amino-N,N,N′,N′-tetramethylisophthalamide

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Technology Process of 2-amino-N,N,N′,N′-tetramethylisophthalamide

There total 5 articles about 2-amino-N,N,N′,N′-tetramethylisophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 57053-08-4
N,N,N',N'-tetramethyl-2-nitroisophthalamide

: 57053-10-8
2-amino-N,N,N′,N′-tetramethylisophthalamide

Guidance literature:: With iron; ammonium chloride; In water; isopropyl alcohol; for 22.5h; Reflux;
DOI:10.1021/om500978n

Reference yield:

: 81-20-9
2,6-dimethylnitrobenzene

: 57053-10-8
2-amino-N,N,N′,N′-tetramethylisophthalamide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide; potassium permanganate

2: thionyl chloride / dichloromethane

3: water; tetrahydrofuran / 1 h / 0 - 20 °C

4: iron; ammonium chloride / water; isopropyl alcohol / 22.5 h / Reflux

With potassium permanganate; thionyl chloride; iron; ammonium chloride; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; isopropyl alcohol;
DOI:10.1021/om500978n

Reference yield:

: 57053-00-6
2-nitro-1,3-benzenedicarbonyl chloride

: 57053-10-8
2-amino-N,N,N′,N′-tetramethylisophthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: water; tetrahydrofuran / 1 h / 0 - 20 °C

2: iron; ammonium chloride / water; isopropyl alcohol / 22.5 h / Reflux

With iron; ammonium chloride; In tetrahydrofuran; water; isopropyl alcohol;
DOI:10.1021/om500978n