C₃₉H₄₄O₁₀

Base Information

Chemical Name:C₃₉H₄₄O₁₀
CAS No.:1315568-00-3
Molecular Formula:C₃₉H₄₄O₁₀
Molecular Weight:672.772
Hs Code.:

C<sub>39</sub>H<sub>44</sub>O<sub>10</sub>

Synonyms:C₃₉H₄₄O₁₀

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Chemical Property of C₃₉H₄₄O₁₀

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Technology Process of C₃₉H₄₄O₁₀

There total 23 articles about C₃₉H₄₄O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1315567-81-7
C₄₅H₅₈O₁₀Si

: 1315568-00-3
C₃₉H₄₄O₁₀

Guidance literature:: With tris(dimethylamino)sulfonium trimethylsilyldifluoride; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1038/nchem.1074

Reference yield:

: 1315567-64-6
C₄₄H₄₈O₁₂

: 1315568-00-3
C₃₉H₄₄O₁₀

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate / methanol; water / 50 °C

1.2: 0 °C

2.1: 2,6-dimethylpyridine; trifluoromethylsulfonic anhydride / dichloromethane / -78 °C

2.2: 65 °C

3.1: ammonium chloride; zinc / ethanol / 160 °C / Microwave irradiation

4.1: pyridinium p-toluenesulfonate / dichloromethane / 40 °C

5.1: N-Bromosuccinimide; sodium hydrogencarbonate; dibenzoyl peroxide / tetrachloromethane; benzene / 70 °C

5.2: 20 °C

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

7.1: dmap; triethylamine / dichloromethane / 20 °C

8.1: toluene-4-sulfonic acid / methanol; N,N-dimethyl-formamide / 200 °C / Microwave irradiation

9.1: dmap / dichloromethane / 20 °C

10.1: tris(dimethylamino)sulfonium trimethylsilyldifluoride / N,N-dimethyl-formamide / 20 °C

With 2,6-dimethylpyridine; dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; trifluoromethylsulfonic anhydride; tris(dimethylamino)sulfonium trimethylsilyldifluoride; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium carbonate; ammonium chloride; toluene-4-sulfonic acid; triethylamine; zinc; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; benzene;
DOI:10.1038/nchem.1074

Reference yield:

: 1315567-79-3
C₃₂H₅₀O₁₀Si

: 1315568-00-3
C₃₉H₄₄O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

2: dmap; triethylamine / dichloromethane / 20 °C

3: toluene-4-sulfonic acid / methanol; N,N-dimethyl-formamide / 200 °C / Microwave irradiation

4: dmap / dichloromethane / 20 °C

5: tris(dimethylamino)sulfonium trimethylsilyldifluoride / N,N-dimethyl-formamide / 20 °C

With dmap; lithium aluminium tetrahydride; tris(dimethylamino)sulfonium trimethylsilyldifluoride; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1038/nchem.1074