C₅₅H₆₉N₉O₁₄S

Base Information

Chemical Name:C₅₅H₆₉N₉O₁₄S
CAS No.:1389332-42-6
Molecular Formula:C₅₅H₆₉N₉O₁₄S
Molecular Weight:1112.27
Hs Code.:

C<sub>55</sub>H<sub>69</sub>N<sub>9</sub>O<sub>14</sub>S

Synonyms:C₅₅H₆₉N₉O₁₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₅H₆₉N₉O₁₄S

Chemical Property:

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Technology Process of C₅₅H₆₉N₉O₁₄S

There total 8 articles about C₅₅H₆₉N₉O₁₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂HF₃O₂*C₃₉H₅₀N₈O₉S

: 5545-52-8
Z-D(tBu)-OH

: 1389332-42-6
C₅₅H₆₉N₉O₁₄S

Guidance literature:: Z-D(tBu)-OH; With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Inert atmosphere;

C₂HF₃O₂*C₃₉H₅₀N₈O₉S; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201200457

Reference yield:

: 1389332-16-4
C₂₀H₂₇N₃O₆

: 1389332-42-6
C₅₅H₆₉N₉O₁₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

2.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: dichloromethane / 2 h / 20 °C / Inert atmosphere

4.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

4.2: 0 - 20 °C / Inert atmosphere

With 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201200457

Reference yield:

: C₂HF₃O₂*C₁₆H₂₁N₅O₅

: 1389332-42-6
C₅₅H₆₉N₉O₁₄S

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 5 h / 20 °C / Inert atmosphere

2.1: palladium on activated charcoal; hydrogen / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

3.1: tetrahydrofuran / 20 °C / Inert atmosphere

4.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

5.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

5.2: 0 - 20 °C / Inert atmosphere

6.1: dichloromethane / 2 h / 20 °C / Inert atmosphere

7.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

7.2: 0 - 20 °C / Inert atmosphere

With 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; palladium on activated charcoal; hydrogen; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1002/chem.201200457