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C22H36O4Si

Base Information
  • Chemical Name:C22H36O4Si
  • CAS No.:936642-20-5
  • Molecular Formula:C22H36O4Si
  • Molecular Weight:392.611
  • Hs Code.:
C<sub>22</sub>H<sub>36</sub>O<sub>4</sub>Si

Synonyms:C22H36O4Si

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Chemical Property of C22H36O4Si
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Technology Process of C22H36O4Si

There total 2 articles about C22H36O4Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
C20H32SiO2; tert-butyldimethylsiloxyacetaldehyde; chiral chromium(III) imine-phenolate complex; at 20 ℃; for 40h;
With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; for 0.5h; Further stages. Title compound not separated from byproducts.; cooling;
DOI:10.1021/ol0701013
Guidance literature:
DOI:10.1021/ol0701013
Guidance literature:
Multi-step reaction with 2 steps
1: diisobutylaluminum hydride / CH2Cl2 / 1 h / cooling
2: 2,6-lutidine / CH2Cl2 / 2 h / 20 °C
With 2,6-dimethylpyridine; diisobutylaluminium hydride; In dichloromethane;
DOI:10.1021/ol0701013
upstream raw materials:

tert-butyldimethylsiloxyacetaldehyde

C22H38O4Si

Downstream raw materials:

C22H38O4Si

C22H38O4Si

C28H52O4Si2

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