4-dimethyloxiranyl-2-[2-(triisopropylsilanyloxy)-4-(triisopropylsilanyloxymethyl)phenyl]butan-2-ol

Base Information

Chemical Name:4-dimethyloxiranyl-2-[2-(triisopropylsilanyloxy)-4-(triisopropylsilanyloxymethyl)phenyl]butan-2-ol
CAS No.:848566-06-3
Molecular Formula:C₃₃H₆₂O₄Si₂
Molecular Weight:579.024
Hs Code.:

Synonyms:4-dimethyloxiranyl-2-[2-(triisopropylsilanyloxy)-4-(triisopropylsilanyloxymethyl)phenyl]butan-2-ol

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Chemical Property of 4-dimethyloxiranyl-2-[2-(triisopropylsilanyloxy)-4-(triisopropylsilanyloxymethyl)phenyl]butan-2-ol

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Technology Process of 4-dimethyloxiranyl-2-[2-(triisopropylsilanyloxy)-4-(triisopropylsilanyloxymethyl)phenyl]butan-2-ol

There total 7 articles about 4-dimethyloxiranyl-2-[2-(triisopropylsilanyloxy)-4-(triisopropylsilanyloxymethyl)phenyl]butan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 848566-05-2
6-methyl-2-[2-(triisopropylsilanyloxy)-4-(triisopropylsilanyloxymethyl)phenyl]hept-5-en-2-ol

: 848566-06-3
4-dimethyloxiranyl-2-[2-(triisopropylsilanyloxy)-4-(triisopropylsilanyloxymethyl)phenyl]butan-2-ol

Guidance literature:: With disodium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1002/ejoc.200400336

Reference yield:

: 2270-59-9
1-bromo-4-methylpent-3-ene

: 848566-06-3
4-dimethyloxiranyl-2-[2-(triisopropylsilanyloxy)-4-(triisopropylsilanyloxymethyl)phenyl]butan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / Mg / diethyl ether / 2 h / Heating

2: 87 percent / Na₂HPO₄; m-CPBA / tetrahydrofuran / 12 h / 20 °C

With disodium hydrogenphosphate; magnesium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether;
DOI:10.1002/ejoc.200400336

Reference yield:

: 13154-24-0
triisopropylsilyl chloride

: 848566-06-3
4-dimethyloxiranyl-2-[2-(triisopropylsilanyloxy)-4-(triisopropylsilanyloxymethyl)phenyl]butan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / imidazole / dimethylformamide / 12 h / 20 °C

2: 74 percent / Mg / diethyl ether / 2 h / Heating

3: 87 percent / Na₂HPO₄; m-CPBA / tetrahydrofuran / 12 h / 20 °C

With 1H-imidazole; disodium hydrogenphosphate; magnesium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200400336