1--4-methyl-2,6,7-trioxabicyclo<2.2.2>octane

Base Information

Chemical Name:1--4-methyl-2,6,7-trioxabicyclo<2.2.2>octane
CAS No.:148150-70-3
Molecular Formula:C₂₉H₂₇NO₆
Molecular Weight:485.536
Hs Code.:

1-<N-(9-fluorenylmethyloxycarbonyl)-(1S)-1-amino-2-phenyl-2-oxoethyl>-4-methyl-2,6,7-trioxabicyclo<2.2.2>octane

Synonyms:1--4-methyl-2,6,7-trioxabicyclo<2.2.2>octane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1--4-methyl-2,6,7-trioxabicyclo<2.2.2>octane

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Technology Process of 1--4-methyl-2,6,7-trioxabicyclo<2.2.2>octane

There total 1 articles about 1--4-methyl-2,6,7-trioxabicyclo<2.2.2>octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: [(S)-2-Hydroxy-1-(4-methyl-2,6,7-trioxa-bicyclo[2.2.2]oct-1-yl)-2-phenyl-ethyl]-carbamic acid 9H-fluoren-9-ylmethyl ester

: 148150-70-3
1--4-methyl-2,6,7-trioxabicyclo<2.2.2>octane

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 2.16667h;

Reference yield:

: 148150-70-3
1--4-methyl-2,6,7-trioxabicyclo<2.2.2>octane

: 32946-42-2
(2S,3S)-2-amino-3-hydroxy-3-phenylpropanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: LiBH₄, CH₃OH / CH₂Cl₂ / 7 h / -78 °C

2: 52 percent / TMSI / 24 h / 75 °C

With methanol; lithium borohydride; trimethylsilyl iodide; In dichloromethane;