10,10-dimethyl-9-(N,N-diphenylureido)-9,10-dihydro-10-sila-2-azaanthracene

Base Information

Chemical Name:10,10-dimethyl-9-(N,N-diphenylureido)-9,10-dihydro-10-sila-2-azaanthracene
CAS No.:122637-93-8
Molecular Formula:C₂₇H₂₅N₃OSi
Molecular Weight:435.601
Hs Code.:

Synonyms:10,10-dimethyl-9-(N,N-diphenylureido)-9,10-dihydro-10-sila-2-azaanthracene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10,10-dimethyl-9-(N,N-diphenylureido)-9,10-dihydro-10-sila-2-azaanthracene

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Technology Process of 10,10-dimethyl-9-(N,N-diphenylureido)-9,10-dihydro-10-sila-2-azaanthracene

There total 2 articles about 10,10-dimethyl-9-(N,N-diphenylureido)-9,10-dihydro-10-sila-2-azaanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 122637-89-2
10,10-dimethyl-9-phenylamino-9,10-dihydro-10-sila-2-azaanthracene

: 103-71-9
phenyl isocyanate

: 122637-93-8
10,10-dimethyl-9-(N,N-diphenylureido)-9,10-dihydro-10-sila-2-azaanthracene

Guidance literature:: With triethylamine; In benzene; for 5h; Heating;
DOI:10.1007/BF00472632

Reference yield:

: 122637-86-9,122637-95-0
10,10-dimethyl-9-phenylimino-10-sila-2-azaanthracene

: 122637-93-8
10,10-dimethyl-9-(N,N-diphenylureido)-9,10-dihydro-10-sila-2-azaanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / Li / diethyl ether / 2 h / Heating

2: 80 percent / Et₃N / benzene / 5 h / Heating

With lithium; triethylamine; In diethyl ether; benzene;
DOI:10.1007/BF00472632