Technology Process of 11-bromoundecan-2-one
There total 1 articles about 11-bromoundecan-2-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; oxygen; copper(l) chloride;
In
tetrahydrofuran;
at 20 ℃;
for 36h;
under 759.826 Torr;
DOI:10.1002/cctc.201500241
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium azide / N,N-dimethyl-formamide / 17 h / 20 °C
2: triethylphosphite copper(I) iodide complex / toluene / Inert atmosphere; Reflux
With
sodium azide; triethylphosphite copper(I) iodide complex;
In
N,N-dimethyl-formamide; toluene;
DOI:10.1039/c2ob06802h
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 38.8 g / Na, NaI / ethanol / 14 h / Heating
2: 90 percent / baryte hydrate / H2O / 24 h / Heating
3: 1.) O3, 2.) Zn,AcOH / 1.) CH2Cl2, 12 min, -78 deg C 2.) r.t
4: 85 percent / Na / ethanol; tetrahydrofuran / 12 h / Ambient temperature
5: H2 / Pd/C / ethanol / 12 h / 2280 Torr / Ambient temperature
6: benzene
With
barium sulfate; Zn,AcOH; hydrogen; sodium; ozone; sodium iodide; zinc;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; water; benzene;
