Bromo-acetic acid (1S,4R)-4-(4-methoxy-phenoxy)-1-methyl-5-oxo-pentyl ester

Base Information

Chemical Name:Bromo-acetic acid (1S,4R)-4-(4-methoxy-phenoxy)-1-methyl-5-oxo-pentyl ester
CAS No.:197907-47-4
Molecular Formula:C₁₅H₁₉BrO₅
Molecular Weight:359.217
Hs Code.:

Synonyms:Bromo-acetic acid (1S,4R)-4-(4-methoxy-phenoxy)-1-methyl-5-oxo-pentyl ester

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Chemical Property of Bromo-acetic acid (1S,4R)-4-(4-methoxy-phenoxy)-1-methyl-5-oxo-pentyl ester

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Technology Process of Bromo-acetic acid (1S,4R)-4-(4-methoxy-phenoxy)-1-methyl-5-oxo-pentyl ester

There total 1 articles about Bromo-acetic acid (1S,4R)-4-(4-methoxy-phenoxy)-1-methyl-5-oxo-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 192992-65-7
Bromo-acetic acid (1S,4R)-5,5-diethoxy-4-(4-methoxy-phenoxy)-1-methyl-pentyl ester

: 197907-47-4
Bromo-acetic acid (1S,4R)-4-(4-methoxy-phenoxy)-1-methyl-5-oxo-pentyl ester

Guidance literature:: With formic acid; In dichloromethane; Ambient temperature;
DOI:10.1016/S0957-4166(97)00339-X

Reference yield: 75.0%

: 197907-47-4
Bromo-acetic acid (1S,4R)-4-(4-methoxy-phenoxy)-1-methyl-5-oxo-pentyl ester

: [(1S,4R)-5,5-Diethoxy-4-(4-methoxy-phenoxy)-1-methyl-pentyloxycarbonylmethyl]-triphenyl-phosphonium; bromide

: (E)-(4S,7S)-7-(2-Bromo-acetoxy)-4-(4-methoxy-phenoxy)-oct-2-enoic acid (1S,4R)-5,5-diethoxy-4-(4-methoxy-phenoxy)-1-methyl-pentyl ester

Guidance literature:: With TEA; In acetonitrile; at 30 ℃;
DOI:10.1016/S0957-4166(97)00339-X

Reference yield:

: 197907-47-4
Bromo-acetic acid (1S,4R)-4-(4-methoxy-phenoxy)-1-methyl-5-oxo-pentyl ester

: (E)-(4S,7S)-7-(2-Bromo-acetoxy)-4-(4-methoxy-phenoxy)-oct-2-enoic acid (1S,4R)-4-(4-methoxy-phenoxy)-1-methyl-5-oxo-pentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / TEA / acetonitrile / 30 °C

2: 100 percent / formic acid / CH₂Cl₂ / Ambient temperature

With formic acid; TEA; In dichloromethane; acetonitrile;
DOI:10.1016/S0957-4166(97)00339-X