(Z)-N-benzyl-3,6-dimethyl-6-(tetrahydro-2H-pyran-2-yloxy)hept-2-en-4-ynamide

Base Information

Chemical Name:(Z)-N-benzyl-3,6-dimethyl-6-(tetrahydro-2H-pyran-2-yloxy)hept-2-en-4-ynamide
CAS No.:1137669-31-8
Molecular Formula:C₂₁H₂₇NO₃
Molecular Weight:341.45
Hs Code.:

Synonyms:(Z)-N-benzyl-3,6-dimethyl-6-(tetrahydro-2H-pyran-2-yloxy)hept-2-en-4-ynamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-N-benzyl-3,6-dimethyl-6-(tetrahydro-2H-pyran-2-yloxy)hept-2-en-4-ynamide

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Technology Process of (Z)-N-benzyl-3,6-dimethyl-6-(tetrahydro-2H-pyran-2-yloxy)hept-2-en-4-ynamide

There total 1 articles about (Z)-N-benzyl-3,6-dimethyl-6-(tetrahydro-2H-pyran-2-yloxy)hept-2-en-4-ynamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 132101-64-5,27943-46-0
3-methyl-3-(tetrahydro-2H-pyran-2-yloxy)butyne

: 601521-86-2
(Z)-N-benzyl-3-iodobut-2-enamide

: 1137669-31-8
(Z)-N-benzyl-3,6-dimethyl-6-(tetrahydro-2H-pyran-2-yloxy)hept-2-en-4-ynamide

Guidance literature:: 3-methyl-3-(tetrahydro-2H-pyran-2-yloxy)butyne; (Z)-N-benzyl-3-iodobut-2-enamide; With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; at 25 ℃; for 4h; Inert atmosphere;

With water; ammonium chloride; In N,N-dimethyl-formamide;
DOI:10.1055/s-0028-1083257

Reference yield:

: 1137669-31-8
(Z)-N-benzyl-3,6-dimethyl-6-(tetrahydro-2H-pyran-2-yloxy)hept-2-en-4-ynamide

: C₂₁H₂₆INO₃

: C₂₁H₂₆INO₃

Guidance literature:: (Z)-N-benzyl-3,6-dimethyl-6-(tetrahydro-2H-pyran-2-yloxy)hept-2-en-4-ynamide; With Iodine monochloride; sodium hydrogencarbonate; In dichloromethane; at 25 ℃; for 4h; Darkness; Inert atmosphere;

With water; sodium thiosulfate; In dichloromethane;
DOI:10.1055/s-0028-1083257

Reference yield:

: 1137669-31-8
(Z)-N-benzyl-3,6-dimethyl-6-(tetrahydro-2H-pyran-2-yloxy)hept-2-en-4-ynamide

: 681842-62-6
(E)-1-benzyl-5-(2-hydroxy-1-iodo-2-methylpropylidene)-4-methyl-1,5-dihydro-2H-pyrrol-2-one

: (Z)-1-benzyl-5-(2-hydroxy-1-iodo-2-methylpropylidene)-4-methyl-1,5-dihydro-2H-pyrrol-2-one

Guidance literature:: (Z)-N-benzyl-3,6-dimethyl-6-(tetrahydro-2H-pyran-2-yloxy)hept-2-en-4-ynamide; With Iodine monochloride; sodium hydrogencarbonate; In dichloromethane; at 25 ℃; for 4h; Darkness; Inert atmosphere;

With water; sodium thiosulfate; In dichloromethane;

With silica gel; In diethyl ether; triethylamine; Petroleum ether; optical yield given as %de;
DOI:10.1055/s-0028-1083257