Benzyl-[1-(6-butyl-3,9-dimethoxy-5,6-dihydro-indolo[2,1-a]isoquinolin-12-yl)-meth-(E)-ylidene]-amine

Base Information

• Chemical Name: Benzyl-[1-(6-butyl-3,9-dimethoxy-5,6-dihydro-indolo[2,1-a]isoquinolin-12-yl)-meth-(E)-ylidene]-amine
• CAS No.: 195731-02-3
• Molecular Formula: C₃₀H₃₂N₂O₂
• Molecular Weight: 452.596

Synonyms:Benzyl-[1-(6-butyl-3,9-dimethoxy-5,6-dihydro-indolo[2,1-a]isoquinolin-12-yl)-meth-(E)-ylidene]-amine

Chemical Property of Benzyl-[1-(6-butyl-3,9-dimethoxy-5,6-dihydro-indolo[2,1-a]isoquinolin-12-yl)-meth-(E)-ylidene]-amine

Chemical Property:

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Technology Process of Benzyl-[1-(6-butyl-3,9-dimethoxy-5,6-dihydro-indolo[2,1-a]isoquinolin-12-yl)-meth-(E)-ylidene]-amine

There total 2 articles about Benzyl-[1-(6-butyl-3,9-dimethoxy-5,6-dihydro-indolo[2,1-a]isoquinolin-12-yl)-meth-(E)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

6-Butyl-3,9-dimethoxy-5,6-dihydro-indolo[2,1-a]isoquinoline-12-carbaldehyde (143398-85-0) + benzylamine (100-46-9) → Benzyl-[1-(6-butyl-3,9-dimethoxy-5,6-dihydro-indolo[2,1-a]isoquinolin-12-yl)-meth-(E)-ylidene]-amine (195731-02-3)

Guidance literature:

With calcium sulfate; acetic acid; In ethanol;

DOI:10.1021/jm970177c

Reference yield:

6-Butyl-3,9-dimethoxy-5,6-dihydro-indolo[2,1-a]isoquinoline (143398-76-9) → Benzyl-[1-(6-butyl-3,9-dimethoxy-5,6-dihydro-indolo[2,1-a]isoquinolin-12-yl)-meth-(E)-ylidene]-amine (195731-02-3)

Guidance literature:

Multi-step reaction with 2 steps

1: POCl₃

2: 80 percent / CaSO₄, AcOH / ethanol

With calcium sulfate; acetic acid; trichlorophosphate; In ethanol;

DOI:10.1021/jm970177c

Reference yield: 73.0%

Benzyl-[1-(6-butyl-3,9-dimethoxy-5,6-dihydro-indolo[2,1-a]isoquinolin-12-yl)-meth-(E)-ylidene]-amine (195731-02-3) → Benzyl-(6-butyl-3,9-dimethoxy-5,6-dihydro-indolo[2,1-a]isoquinolin-12-ylmethyl)-amine

Guidance literature:

With sodium tetrahydroborate; In methanol; a) RT, 1 h, b) reflux, 45 min;

DOI:10.1021/jm970177c

upstream raw materials:

6-Butyl-3,9-dimethoxy-5,6-dihydro-indolo[2,1-a]isoquinoline-12-carbaldehyde

benzylamine

6-Butyl-3,9-dimethoxy-5,6-dihydro-indolo[2,1-a]isoquinoline

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