N-(2,3-Dichlorophenyl)-2-hydroxy-4-oxo-1,5-dioxaspiro(5.5)undec-2-ene-3-carboxamide

Base Information

Chemical Name:N-(2,3-Dichlorophenyl)-2-hydroxy-4-oxo-1,5-dioxaspiro(5.5)undec-2-ene-3-carboxamide
CAS No.:150379-37-6
Molecular Formula:C₁₆H₁₅Cl₂NO₅
Molecular Weight:372.205
Hs Code.:
DSSTox Substance ID:DTXSID00164535
Nikkaji Number:J611.605A
Wikidata:Q83033598
Mol file:150379-37-6.mol

Synonyms:2-hydroxy-4-oxo-1,5-dioxaspiro(5,5)undec-2-ene-3-N-(2,4-dichlorophenyl)carboxamide;CGP 43182;CGP-43182;CGP43182

Suppliers and Price of N-(2,3-Dichlorophenyl)-2-hydroxy-4-oxo-1,5-dioxaspiro(5.5)undec-2-ene-3-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of N-(2,3-Dichlorophenyl)-2-hydroxy-4-oxo-1,5-dioxaspiro(5.5)undec-2-ene-3-carboxamide

Chemical Property:

Vapor Pressure:7.34E-14mmHg at 25°C
Boiling Point:570.6°C at 760 mmHg
Flash Point:298.9°C
Density:1.53g/cm³
XLogP3:4.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:371.0327280
Heavy Atom Count:24
Complexity:559

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC2(CC1)OC(=C(C(=O)O2)C(=O)NC3=C(C(=CC=C3)Cl)Cl)O

Technology Process of N-(2,3-Dichlorophenyl)-2-hydroxy-4-oxo-1,5-dioxaspiro(5.5)undec-2-ene-3-carboxamide

There total 3 articles about N-(2,3-Dichlorophenyl)-2-hydroxy-4-oxo-1,5-dioxaspiro(5.5)undec-2-ene-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1658-27-1
1,5-dioxaspiro[5.5]undecane-2,4-dione

: 41195-90-8
1,2-dichloro-3-isocyanatobenzene

: 150379-37-6
2-hydroxy-4-oxo-1,5-dioxaspiro<5.5>undec-2-ene-3-N-(2,3-dichlorophenyl)-carboxamide

Guidance literature:: With triethylamine; In acetone; for 14h; Ambient temperature;
DOI:10.1016/0223-5234(94)90026-4

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 150379-37-6
2-hydroxy-4-oxo-1,5-dioxaspiro<5.5>undec-2-ene-3-N-(2,3-dichlorophenyl)-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: Ac₂O, H₂SO₄

2: 32 percent / Et₃N / acetone / 14 h / Ambient temperature

With sulfuric acid; acetic anhydride; triethylamine; In acetone;
DOI:10.1016/0223-5234(94)90026-4

Reference yield:

: 608-27-5
2,3-dichloroaniline

: 150379-37-6
2-hydroxy-4-oxo-1,5-dioxaspiro<5.5>undec-2-ene-3-N-(2,3-dichlorophenyl)-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: dioxane / 5 h / 100 °C

2: 32 percent / Et₃N / acetone / 14 h / Ambient temperature

With triethylamine; In 1,4-dioxane; acetone;
DOI:10.1016/0223-5234(94)90026-4