C₁₅H₂₆O₂Si

Base Information

Chemical Name:C₁₅H₂₆O₂Si
CAS No.:1332745-33-1
Molecular Formula:C₁₅H₂₆O₂Si
Molecular Weight:266.456
Hs Code.:

C<sub>15</sub>H<sub>26</sub>O<sub>2</sub>Si

Synonyms:C₁₅H₂₆O₂Si

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Chemical Property of C₁₅H₂₆O₂Si

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Technology Process of C₁₅H₂₆O₂Si

There total 1 articles about C₁₅H₂₆O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 18448-47-0
methyl cyclohex-1-ene-1-carboxylate

: 69361-41-7
4-bromo-1-trimethylsilylbut-1-yne

: 1332745-33-1
C₁₅H₂₆O₂Si

Guidance literature:: 4-bromo-1-trimethylsilylbut-1-yne; With iodine; magnesium; In tetrahydrofuran; at 20 ℃; for 0.5h; Reflux; Inert atmosphere;

methyl cyclohex-1-ene-1-carboxylate; With chloro-trimethyl-silane; copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; at -40 ℃; for 8h; Inert atmosphere;
DOI:10.1021/ja206837j

Reference yield:

: 1332745-33-1
C₁₅H₂₆O₂Si

: C₂₀H₂₃NO₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 °C / Inert atmosphere

2.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 20 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

4.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

5.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 6 h / 80 °C / Inert atmosphere

6.1: sodium tetrachloroaurate (III) hydrate / dichloromethane / 6 h / 20 °C / Inert atmosphere

7.1: silver hexafluoroantimonate; chloro(1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene)gold(I) / dichloromethane / 0.9 h / 20 °C / Inert atmosphere

With silver hexafluoroantimonate; lithium hydroxide monohydrate; sodium tetrachloroaurate (III) hydrate; chloro(1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene)gold(I); potassium hexamethylsilazane; sodium hydrogencarbonate; Dess-Martin periodane; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1021/ja206837j

Reference yield:

: 1332745-33-1
C₁₅H₂₆O₂Si

: C₂₀H₂₅NO₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 °C / Inert atmosphere

2.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 20 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

4.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

5.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 6 h / 80 °C / Inert atmosphere

6.1: silver hexafluoroantimonate; chloro(1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene)gold(I) / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

With silver hexafluoroantimonate; lithium hydroxide monohydrate; chloro(1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene)gold(I); potassium hexamethylsilazane; sodium hydrogencarbonate; Dess-Martin periodane; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1021/ja206837j