C₂₄H₃₁N₃O₅S

Base Information

Chemical Name:C₂₄H₃₁N₃O₅S
CAS No.:1309766-23-1
Molecular Formula:C₂₄H₃₁N₃O₅S
Molecular Weight:473.593
Hs Code.:

C<sub>24</sub>H<sub>31</sub>N<sub>3</sub>O<sub>5</sub>S

Synonyms:C₂₄H₃₁N₃O₅S

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Chemical Property of C₂₄H₃₁N₃O₅S

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Technology Process of C₂₄H₃₁N₃O₅S

There total 4 articles about C₂₄H₃₁N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1309766-32-2
C₁₇H₂₄BrN₃O₃

: 149104-88-1
4-methanesulphonylphenylboronic acid

: 1309766-23-1
C₂₄H₃₁N₃O₅S

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water; at 90 ℃; for 24h; Sealed tube;

Reference yield:

: 273376-39-9
tert-butyl rel-(1R,3r,5S)-3-(hydroxymethyl)-8-azabicyclo[3.2.1]octane-8-carboxylate

: 1309766-23-1
C₂₄H₃₁N₃O₅S

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium t-butanolate / tetrahydrofuran / 0.25 h / 20 °C

1.2: 17 h / 60 °C

2.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 24 h / 90 °C / Sealed tube

With potassium carbonate; sodium t-butanolate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; water; 2.1: Suzuki Coupling;

Reference yield:

: 185099-67-6
N-Boc-nortropinone

: 1309766-23-1
C₂₄H₃₁N₃O₅S

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C

2.1: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran / 0 - 20 °C

2.2: 50 °C

3.1: sodium t-butanolate / tetrahydrofuran / 0.25 h / 20 °C

3.2: 17 h / 60 °C

4.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 24 h / 90 °C / Sealed tube

With sodium tetrahydroborate; boron trifluoride diethyl etherate; potassium tert-butylate; potassium carbonate; sodium t-butanolate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; water; 4.1: Suzuki Coupling;